Benzenemethanol, a-ethenyl-2-hydroxy-

Base Information

• Chemical Name: Benzenemethanol, a-ethenyl-2-hydroxy-
• CAS No.: 38865-40-6
• Molecular Formula: C9H10O2
• Molecular Weight: 150.177
• Mol file: 38865-40-6.mol

Synonyms:o-(1-hydroxyallyl)phenol;2-(1-hydroxyallyl)phenol;1-(o-Hydroxyphenyl)-2-propen-1-ol;1-(2-Hydroxyphenyl)-2-propen-1-ol;

Chemical Property of Benzenemethanol, a-ethenyl-2-hydroxy-

Chemical Property:

• PSA: 40.46000
• LogP: 1.61160

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, a-ethenyl-2-hydroxy-

There total 9 articles about Benzenemethanol, a-ethenyl-2-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

vinylmagnesium chloride (3536-96-7) + salicylaldehyde (90-02-8) → 1-(2'-hydroxyphenyl)prop-2-en-1-ol (38865-40-6)

Guidance literature:

In tetrahydrofuran; at -78 - 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/adsc.201500058

Reference yield: 89.0%

vinyl magnesium bromide (1826-67-1) + salicylaldehyde (90-02-8) → 1-(2'-hydroxyphenyl)prop-2-en-1-ol (38865-40-6)

Guidance literature:

In tetrahydrofuran;

DOI:10.1002/ejoc.201200770

Reference yield:

1-(2-((tert-butyldimethylsilyl)oxy)phenyl)prop-2-en-1-ol → 1-(2'-hydroxyphenyl)prop-2-en-1-ol (38865-40-6)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmcl.2005.01.070

upstream raw materials:

vinyl magnesium bromide

salicylaldehyde

2-hydroxybromobenzene

acrolein

Downstream raw materials:

5-(2'-hydroxyphenyl)tetrahydrofuran-2-ol

2-[2-(1-hydroxyprop-2-en-1-yl)phenoxy]acetonitrile