2-{[(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO}BENZOIC ACID

Base Information

Chemical Name:2-{[(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO}BENZOIC ACID
CAS No.:22780-32-1
Molecular Formula:C17H15 N O4
Molecular Weight:297.31
Hs Code.:2924299090
Mol file:22780-32-1.mol

Synonyms:Anthranilicacid, N-(p-methoxycinnamoyl)- (8CI); Benzoic acid,2-[[3-(4-methoxyphenyl)-1-oxo-2-propenyl]amino]- (9CI);N-(4-Methoxycinnamoyl)anthranilic acid

Suppliers and Price of 2-{[(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO}BENZOIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-([(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO)BENZOIC ACID 95.00%
5G
$ 1005.43

American Custom Chemicals Corporation
2-([(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO)BENZOIC ACID 95.00%
2.5G
$ 852.21

American Custom Chemicals Corporation
2-([(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO)BENZOIC ACID 95.00%
1G
$ 648.81

Total 2 raw suppliers

Chemical Property of 2-{[(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO}BENZOIC ACID

Chemical Property:

Vapor Pressure:7.32E-14mmHg at 25°C
Boiling Point:570.7°Cat760mmHg
Flash Point:298.9°C
PSA：75.63000
Density:g/cm³
LogP:3.11830

Purity/Quality:

99% ^*data from raw suppliers

2-([(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO)BENZOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-{[(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO}BENZOIC ACID

There total 5 articles about 2-{[(2E)-3-(4-METHOXYPHENYL)PROP-2-ENOYL]AMINO}BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 53947-84-5
2-[(2-carboxyacetyl)amino]benzoic acid

: 123-11-5
4-methoxy-benzaldehyde

: 22780-32-1
N-(4-methoxycinnamoyl)anthranilic acid

Guidance literature:: 2-[(2-carboxyacetyl)amino]benzoic acid; 4-methoxy-benzaldehyde; With piperidine; In toluene; for 3h; Reflux; Dean-Stark;

With methanol; In water; at 40 ℃;

With hydrogenchloride; In water;
DOI:10.1016/j.ejmech.2019.02.074

Reference yield: 40.0%

: 123-11-5
4-methoxy-benzaldehyde

: 89-52-1
o-acetylamino-benzoic acid

: 22780-32-1
N-(4-methoxycinnamoyl)anthranilic acid

Guidance literature:: With sodium hydroxide; In methanol; Heating;

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 22780-32-1
N-(4-methoxycinnamoyl)anthranilic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / CHCl₃ / 2 h / 0 - 5 °C

2: 40 percent / NaOH / methanol / Heating

With sodium hydroxide; In methanol; chloroform;