2-Phenylcyclohexanone oxime

Base Information

Chemical Name:2-Phenylcyclohexanone oxime
CAS No.:22591-17-9
Molecular Formula:C12H15 N O
Molecular Weight:189.257
Hs Code.:2928000090
NSC Number:122965
DSSTox Substance ID:DTXSID20421056
Nikkaji Number:J83.196D
Mol file:22591-17-9.mol

Synonyms:2-phenylcyclohexanone oxime;22591-17-9;NSC122965;(NZ)-N-(2-phenylcyclohexylidene)hydroxylamine;DTXSID20421056;AKOS024324806;NSC-122965

Suppliers and Price of 2-Phenylcyclohexanone oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2-PHENYLCYCLOHEXANONE OXIME Aldrich
1ea
$ 57.00

American Custom Chemicals Corporation
2-PHENYLCYCLOHEXANONE OXIME 95.00%
5MG
$ 504.47

Total 2 raw suppliers

Chemical Property of 2-Phenylcyclohexanone oxime

Chemical Property:

Vapor Pressure:3.48E-05mmHg at 25°C
Boiling Point:339.8°C at 760 mmHg
Flash Point:210.7°C
PSA：32.59000
Density:1.1g/cm³
LogP:3.17440
XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:189.115364102
Heavy Atom Count:14
Complexity:206

Purity/Quality:: 2-PHENYLCYCLOHEXANONE OXIME Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=NO)C(C1)C2=CC=CC=C2
Isomeric SMILES:C1CC/C(=N/O)/C(C1)C2=CC=CC=C2

Technology Process of 2-Phenylcyclohexanone oxime

There total 5 articles about 2-Phenylcyclohexanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1444-65-1
(RS)-2-phenylcyclohexanone

: 22591-17-9
(R,S)-(E)-2-phenylcyclohexanone oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In methanol; water; at 60 ℃;
DOI:10.1021/jo00128a009

Reference yield:

: 1444-65-1
(RS)-2-phenylcyclohexanone

: 5470-11-1
hydroxylamine hydrochloride

: 22591-17-9
(R,S)-(E)-2-phenylcyclohexanone oxime

Guidance literature:: With potassium carbonate; In ethanol; water;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 22591-17-9
2-phenylcyclohexanone oxime

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; tris-(o-tolyl)phosphine; sodium acetate; pyrrolidine; tert-Octylamine / 1,4-dioxane / 110 °C / Inert atmosphere; Schlenk technique; Sealed tube

2: sodium hydroxide; hydroxylamine hydrochloride / ethanol; water / 20 °C / Inert atmosphere; Schlenk technique

With pyrrolidine; tert-Octylamine; hydroxylamine hydrochloride; sodium acetate; palladium diacetate; tris-(o-tolyl)phosphine; sodium hydroxide; In 1,4-dioxane; ethanol; water;
DOI:10.1002/cjoc.201800206