4-benzoylbenzoyl Chloride

Base Information

• Chemical Name: 4-benzoylbenzoyl Chloride
• CAS No.: 39148-58-8
• Molecular Formula: C14H9ClO2
• Molecular Weight: 244.677
• DSSTox Substance ID: DTXSID60512775
• Nikkaji Number: J2.060.752A
• Wikidata: Q82372166
• Mol file: 39148-58-8.mol

Synonyms:4-benzoylbenzoyl Chloride;39148-58-8;4-benzoylbenzoylchloride;4-benzoyl-benzoyl chloride;p-benzoylbenzoylchloride;4-chloroformylbenzophenone;4-benzoyl benzoic chloride;4- Benzoylbenzoyl Chloride;4-(Benzoyl)benzoyl Chloride;SCHEMBL82788;p-benzoylbenzoic acid chloride;para-benzoylbenzoic acid chloride;DTXSID60512775;OZCULFZQSHFJNI-UHFFFAOYSA-N;para-benzoyl benzoic acid chloride

Chemical Property of 4-benzoylbenzoyl Chloride

Chemical Property:

• PSA: 34.14000
• LogP: 3.29660
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 244.0291072
• Heavy Atom Count: 17
• Complexity: 287

Purity/Quality:

99% ^*data from raw suppliers

BENZOYL CHLORIDE,4-BENZOYL- 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)C2=CC=C(C=C2)C(=O)Cl

Technology Process of 4-benzoylbenzoyl Chloride

There total 7 articles about 4-benzoylbenzoyl Chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.1%

4-carboxybenzophenone (611-95-0) → 4-benzoylbenzoyl chloride (39148-58-8)

Guidance literature:

With phosphorus pentachloride; In diethyl ether;

DOI:10.1021/jm00061a001

Reference yield:

oxalyl dichloride (79-37-8) + 4-carboxybenzophenone (611-95-0) → 4-benzoylbenzoyl chloride (39148-58-8)

Guidance literature:

With N,N-dimethyl-formamide; In tetrahydrofuran; at 120 ℃; for 1h;

Reference yield:

4-Methylbenzophenone (134-84-9) → 4-benzoylbenzoyl chloride (39148-58-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium dichromate

2: phosphorous pentachloride

With sodium dichromate; phosphorus pentachloride;

DOI:10.1080/00268948208072592

upstream raw materials:

4-carboxybenzophenone

4-Methylbenzophenone

phosgene

benzyltrimethylammonium chloride

Downstream raw materials:

4-diazoacetyl-benzophenone

4-benzoyl-benzoic acid dimethylamide

4-benzoyl-benzoic acid-(2-diethylamino-ethyl ester)

n-dodecyl benzophenone-4-carboxylate