3-Phenoxypyridin-2-amine

Base Information

• Chemical Name: 3-Phenoxypyridin-2-amine
• CAS No.: 391906-83-5
• Molecular Formula: C11H10N2O
• Molecular Weight: 186.213
• European Community (EC) Number: 848-240-2
• Nikkaji Number: J1.505.400J
• Mol file: 391906-83-5.mol

Synonyms:3-phenoxypyridin-2-amine;391906-83-5;3-Phenoxy-2-pyridinamine;2-Pyridinamine, 3-phenoxy-;phenoxy-amino-pyridine;SCHEMBL1327928;MJTHRNDBNYACBS-UHFFFAOYSA-N;MFCD20693745;AKOS025396374;DS-8594;SB52527;CS-0156076;A918803

Chemical Property of 3-Phenoxypyridin-2-amine

Chemical Property:

• PSA: 48.14000
• LogP: 3.03730
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C
• XLogP3: 2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 186.079312947
• Heavy Atom Count: 14
• Complexity: 169

Purity/Quality:

97% ^*data from raw suppliers

3-Phenoxypyridin-2-amine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)OC2=C(N=CC=C2)N

Technology Process of 3-Phenoxypyridin-2-amine

There total 8 articles about 3-Phenoxypyridin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-Amino-3-bromopyridine (13534-99-1) + phenol (108-95-2,27073-41-2) → 2-amino-3-phenoxypyridine (391906-83-5)

Guidance literature:

With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 90 ℃; Inert atmosphere;

Reference yield: 87.1%

3-(2,4-dibromophenoxy)pyridin-2-amine (1065607-12-6) → 2-amino-3-phenoxypyridine (391906-83-5)

Guidance literature:

With hydrogen; sodium acetate; In ethanol; for 24h; under 1810.07 Torr;

DOI:10.1016/j.bmc.2019.115232

Reference yield: 83.0%

2-nitro-3-phenoxy-pyridine → 2-amino-3-phenoxypyridine (391906-83-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 12h;

DOI:10.1055/s-2001-18103

upstream raw materials:

3-fuoro-2-nitropyridine

phenol

3-(2,4-dibromophenoxy)pyridin-2-amine

2-amino-3-hydroxypyridine

Downstream raw materials:

5-bromo-3-phenoxypyridin-2-amine

5-bromo-N-(4-methylthiazol-2-yl)-3-phenoxypyridin-2-amine

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