Butanamide, 3-amino-N-cyclohexyl-2-hydroxy-

Base Information

Chemical Name:Butanamide, 3-amino-N-cyclohexyl-2-hydroxy-
CAS No.:395644-86-7
Molecular Formula:C10H20N2O2
Molecular Weight:200.281
Hs Code.:

Synonyms:

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Chemical Property of Butanamide, 3-amino-N-cyclohexyl-2-hydroxy-

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Technology Process of Butanamide, 3-amino-N-cyclohexyl-2-hydroxy-

There total 4 articles about Butanamide, 3-amino-N-cyclohexyl-2-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 395644-83-4
N-cyclohexyl-2-hydroxy-3-nitrobutyric amide

: 395644-86-7
N-cyclohexyl-2-hydroxy-3-aminobutyric amide

Guidance literature:: N-cyclohexyl-2-hydroxy-3-nitrobutyric amide; With formic acid; hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 12h; under 3040 Torr;

With ammonium chloride; zinc; In methanol; at 20 ℃; for 12h;
DOI:10.1055/s-2002-31948

Reference yield:

: 51737-90-7
N-Cyclohexyl-2-oxo-acetamide

: 395644-86-7
N-cyclohexyl-2-hydroxy-3-aminobutyric amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 19.0 g / KF/Al₂O₃ / 48 h / 20 °C

2.1: H₂; HCOOH / 10 percent Pd/C; P-2 Ni / methanol / 12 h / 20 °C / 3040 Torr

2.2: Zn; aq. NH₄Cl / methanol / 12 h / 20 °C

With aluminum oxide; potassium fluoride; formic acid; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1055/s-2002-31948

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 395644-86-7
N-cyclohexyl-2-hydroxy-3-aminobutyric amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 76.7 percent / K₂CO₃ / methanol / 7 h / Heating

2.1: H₅IO₆ / ethanol; diethyl ether / 24 h / 20 °C

3.1: 19.0 g / KF/Al₂O₃ / 48 h / 20 °C

4.1: H₂; HCOOH / 10 percent Pd/C; P-2 Ni / methanol / 12 h / 20 °C / 3040 Torr

4.2: Zn; aq. NH₄Cl / methanol / 12 h / 20 °C

With aluminum oxide; potassium fluoride; formic acid; hydrogen; potassium carbonate; periodic acid; palladium on activated charcoal; In methanol; diethyl ether; ethanol;
DOI:10.1055/s-2002-31948