N1,N4-DICYCLOHEXYL-2,3-DIHYDROXYSUCCINAMIDE

Base Information

• Chemical Name: N1,N4-DICYCLOHEXYL-2,3-DIHYDROXYSUCCINAMIDE
• CAS No.: 14445-99-9
• Molecular Formula: C16H28N2O4
• Molecular Weight: 312.4
• Hs Code.: 2924299090
• Mol file: 14445-99-9.mol

Synonyms:N1,N4-DICYCLOHEXYL-2,3-DIHYDROXYSUCCINAMIDE

Chemical Property of N1,N4-DICYCLOHEXYL-2,3-DIHYDROXYSUCCINAMIDE

Chemical Property:

• PSA: 98.66000
• LogP: 1.38780

Purity/Quality:

99% ^*data from raw suppliers

N1,N4-DICYCLOHEXYL-2,3-DIHYDROXYSUCCINAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N1,N4-DICYCLOHEXYL-2,3-DIHYDROXYSUCCINAMIDE

There total 3 articles about N1,N4-DICYCLOHEXYL-2,3-DIHYDROXYSUCCINAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.7%

diethyl (2R,3R)-tartrate (87-91-2) + cyclohexylamine (108-91-8,157973-60-9) → N,N'-dicyclohexyl-2,3-dihydroxysuccinic diamide (14445-99-9)

Guidance literature:

With potassium carbonate; In methanol; for 7h; Heating;

DOI:10.1055/s-2002-31948

Reference yield: 30.0%

L-Tartaric acid (87-69-4,138508-61-9) + cyclohexylamine (108-91-8,157973-60-9) → N,N'-dicyclohexyl-2,3-dihydroxysuccinic diamide (14445-99-9)

Guidance literature:

at 20 - 180 ℃; for 0.2h; microwave irradiation;

DOI:10.1055/s-2001-18724

Reference yield:

dimethyl L-tartrate (608-68-4) + cyclohexylamine (108-91-8,157973-60-9) → N,N'-dicyclohexyl-2,3-dihydroxysuccinic diamide (14445-99-9)

Guidance literature:

at 80 ℃; for 1h; Sealed tube; Inert atmosphere;

upstream raw materials:

L-Tartaric acid

cyclohexylamine

diethyl (2R,3R)-tartrate

dimethyl L-tartrate

Downstream raw materials:

N-benzyl-N'-{[[1-(2-cyclohexylcarbamoyl-2-hydroxy-1-methyl-ethylcarbamoyl)-2-phenyl-ethyl]-(3-methyl-butyl)-carbamoyl]-methyl}-succinamide

N-benzyl-N'-({benzyl-[1-(2-cyclohexylcarbamoyl-2-hydroxy-1-methyl-ethylcarbamoyl)-3-methyl-butyl]-carbamoyl}-methyl)-succinamide

N-benzyl-N'-{[[1-(2-cyclohexylcarbamoyl-2-hydroxy-1-methyl-ethylcarbamoyl)-3-methyl-butyl]-(3-methyl-butyl)-carbamoyl]-methyl}-succinamide

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