Allyl chloromethyl ether

Base Information

• Chemical Name: Allyl chloromethyl ether
• CAS No.: 3970-20-5
• Molecular Formula: C4H7ClO
• Molecular Weight: 106.552
• Hs Code.: 2909199090
• Mol file: 3970-20-5.mol

Synonyms:

Chemical Property of Allyl chloromethyl ether

Chemical Property:

• PSA: 9.23000
• LogP: 1.38530

Purity/Quality:

99%, ^*data from raw suppliers

3-(Chloromethoxy)prop-1-ene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Allyl chloromethyl ether

There total 3 articles about Allyl chloromethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + allyl alcohol (107-18-6) → allyl chloromethyl ether (3970-20-5)

Guidance literature:

With hydrogenchloride; at 0 ℃; for 3h;

DOI:10.1135/cccc2009569

Reference yield:

1,3,5-Trioxan (110-88-3) + allyl alcohol (107-18-6) → allyl chloromethyl ether (3970-20-5)

Guidance literature:

With hydrogenchloride;

DOI:10.1007/BF00961040

Reference yield:

→ allyl chloromethyl ether (3970-20-5)

Guidance literature:

upstream raw materials:

formaldehyd

allyl alcohol

1,3,5-Trioxan

Downstream raw materials:

bis(allyloxy)methane

1-ethoxy-2-allyloxymethoxy-ethane

2-allyloxymethoxy-propionic acid ethyl ester

Allyl-(3-chlor-3-phenyl-propyl)-ether

Refernces

• 1、 Babu, K. Srihari,Rao, M. Raghavendar,Goverdhan,Srinivas,Reddy, P. Pratap,Venkateswarlu,Anand, R. Vijaya. "Synthesis of valganciclovir hydrochloride congeners". . p. 1751 - 1758. Retrieved 2013/05/22.
• 2、 Kawasaki, Takeshi,Kimachi, Tetsutaro. "Sparteine-mediated enantioselective [2,3]-Wittig rearrangement of allyl ortho-substituted benzyl ethers and ortho-substituted benzyl prenyl ethers". . p. 6847 - 6862. Retrieved 2007/10/03.