TERT-BUTYL 4-(4-CHLOROANILINO)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE

Base Information Edit

Chemical Name:TERT-BUTYL 4-(4-CHLOROANILINO)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE
CAS No.:401565-95-5
Molecular Formula:C16H23ClN2O2
Molecular Weight:310.824
Hs Code.:
Mol file:401565-95-5.mol

Synonyms:tert-butyl 4-(4-chlorophenylamino)piperidine-1-carboxylate;tert-butyl 4-(4-chloroanilino)-1-piperidinecarboxylate;4-(4-chloro-phenylamino)-piperidine-1-carboxylic acid tert-butyl ester;TERT-BUTYL 4-(4-CHLOROANILINO)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE;1-(tert-butoxycarbonyl)-4-[(4-chlorophenyl)amino]piperidine;tert-butyl 4-(4-chlorophenylamino)-piperidine-1-carboxylate;tert-butyl 4-((4-chlorophenyl)amino)piperidine-1-carboxylate;

Suppliers and Price of TERT-BUTYL 4-(4-CHLOROANILINO)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
TERT-BUTYL 4-(4-CHLOROANILINO)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE 95.00%
1MG
$ 586.97

Total 2 raw suppliers

Chemical Property of TERT-BUTYL 4-(4-CHLOROANILINO)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE Edit

Chemical Property:

PSA：41.57000
LogP:4.16230

Purity/Quality:

99% ，98% ^*data from raw suppliers

TERT-BUTYL 4-(4-CHLOROANILINO)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of TERT-BUTYL 4-(4-CHLOROANILINO)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE

There total 3 articles about TERT-BUTYL 4-(4-CHLOROANILINO)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 106-47-8
4-chloro-aniline

: 401565-95-5
1-(tert-Butoxycarbonyl)-4-[(4-chlorophenyl)amino]piperidine

Guidance literature:: N-tert-butyloxycarbonylpiperidin-4-one; 4-chloro-aniline; With sodium tris(acetoxy)borohydride; In tetrahydrofuran; at 80 ℃; for 0.166667h; Microwave irradiation;

With water; In tetrahydrofuran;

Reference yield: 65.0%

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 56553-60-7
sodium tris(acetoxy)borohydride

: 106-47-8
4-chloro-aniline

: 401565-95-5
1-(tert-Butoxycarbonyl)-4-[(4-chlorophenyl)amino]piperidine

Guidance literature:: N-tert-butyloxycarbonylpiperidin-4-one; 4-chloro-aniline; With titanium(IV) isopropylate; In 1,2-dichloro-ethane; at 20 ℃; for 14h; Inert atmosphere;

sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 2h; Inert atmosphere;