L-Valine, N-(phenylmethyl)-, methyl ester

Base Information

Chemical Name:L-Valine, N-(phenylmethyl)-, methyl ester
CAS No.:40216-62-4
Molecular Formula:C13H19NO2
Molecular Weight:221.299
Hs Code.:
Mol file:40216-62-4.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-Valine, N-(phenylmethyl)-, methyl ester

Chemical Property:

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Technology Process of L-Valine, N-(phenylmethyl)-, methyl ester

There total 24 articles about L-Valine, N-(phenylmethyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4070-48-8
L-valine methyl ester

: 100-52-7
benzaldehyde

: 40216-62-4
methyl 2-(benzylamino)-3-methylbutanoate

Guidance literature:: With (2,6-dichlorophenyl)bis(2,3,5,6-tetrafluorophenyl)borane; hydrogen; In tetrahydrofuran; at 100 ℃; for 15h; under 60804.1 Torr; Sealed tube; Molecular sieve; Autoclave; Green chemistry;
DOI:10.1021/jacs.8b03626

Reference yield: 90.0%

: 4070-48-8
L-Valine methyl ester

: 100-52-7
benzaldehyde

: 40216-62-4
N-benzyl-L-valine methyl ester

Guidance literature:: With sodium cyanoborohydride; In methanol; acetic acid; for 3h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81078-4

Reference yield: 88.0%

: C₁₃H₁₇NO₂*H⁽¹⁺⁾

: 40216-62-4
N-benzyl-L-valine methyl ester

Guidance literature:: With [Cp*Ir-(4,4’-dimethoxyl-2,2’-bipyridine)(OH₂)][SO₄]; 1-Benzyl-1,4-dihydronicotinamide; In aq. phosphate buffer; at 20 ℃; for 24h; pH=7;
DOI:10.1002/cctc.201601307