Butanedioic acid, bis(trimethylsilyl) ester

Base Information

• Chemical Name: Butanedioic acid, bis(trimethylsilyl) ester
• CAS No.: 40309-57-7
• Molecular Formula: C10H22O4Si2
• Molecular Weight: 262.453
• DSSTox Substance ID: DTXSID10334520
• Nikkaji Number: J47.583A
• Wikidata: Q63399111
• Mol file: 40309-57-7.mol

Synonyms:Butanedioic acid, bis(trimethylsilyl) ester;40309-57-7;Bis(trimethylsilyl) succinate;Succinic acid (tms);bis(trimethylsilyl) butanedioate;Succinate, bis-TMS;Succinic acid, di-TMS;Succinic acid (2TMS);Succinic acid, bis-TMS;Bis(trimethylsilyl)succinate;SCHEMBL4303758;Butanedioic acid, di-TMS ester;DTXSID10334520;Butanedioic acid, 2TMS derivative;succinic acid di(trimethylsilyl) ester;Succinic acid bis(trimethylsilyl) ester;Succinic acid, di(trimethylsilyl) ester;Succinic acid, bis(trimethylsilyl) ester;FT-0701217;BUTANEDIOIC ACID BIS(TRIMETHYLSILYL) ESTER;Q63399111

Chemical Property of Butanedioic acid, bis(trimethylsilyl) ester

Chemical Property:

• PSA: 52.60000
• LogP: 2.52280
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 262.10566225
• Heavy Atom Count: 16
• Complexity: 235

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)OC(=O)CCC(=O)O[Si](C)(C)C

Technology Process of Butanedioic acid, bis(trimethylsilyl) ester

There total 8 articles about Butanedioic acid, bis(trimethylsilyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide (21149-38-2) + formamide (77287-34-4,77287-35-5,60100-09-6) → N,O-bis(trimethylsilyl)-α-alanine (2899-44-7) + 2-methylglyoxylic acid trimethylsilyl ether (52060-85-2) + glycine trimethylsilyl ester (5269-37-4) + N,N'-bis(trimethylsilyl)urea (18297-63-7,127290-39-5) + butanedioic acid bis(trimethylsilyl) ester (40309-57-7) + [(trimethylsilyl)oxy]butanedioic acid bis(trimethylsilyl) ester (65143-63-7,107241-82-7,38166-11-9) + ethanedioic acid bis(trimethylsilyl)ester (18294-04-7) + C11H20N4OSi2 + C9H18N2O3Si2 + C7H21N3Si2 + C13H29N3OSi3 + C8H21N5Si2 + bis(trimethylsilyl)cytosine (67014-25-9) + 7-Trimethylsilylpurin (75773-52-3) + N,N-bis(trimethysilyl)adenine (17995-04-9) + tris(trimethyl)guanine + N-Formyl-N,O-bis(trimethylsilyl)glycine (55517-31-2) + 4-(trimethylsiloxy)pyrimidine (52523-25-8) + 1,3-bis(trimethylsilyl)uracil (3442-82-8)

Guidance literature:

formamide; With water; magnesium sulfate; at 80 ℃; for 24h;

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide; With pyridine; at 60 ℃; for 4h;

DOI:10.1002/chem.201706162

Reference yield:

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide (21149-38-2) + formamide (77287-34-4,77287-35-5,60100-09-6) → N,O-bis(trimethylsilyl)-α-alanine (2899-44-7) + glycine trimethylsilyl ester (5269-37-4) + N,N'-bis(trimethylsilyl)urea (18297-63-7,127290-39-5) + butanedioic acid bis(trimethylsilyl) ester (40309-57-7) + propanoic acid,2-[(trimethylsilyl)oxy] trimethylsilyl ester (17596-96-2) + [(trimethylsilyl)oxy]butanedioic acid bis(trimethylsilyl) ester (65143-63-7,107241-82-7,38166-11-9) + ethanedioic acid bis(trimethylsilyl)ester (18294-04-7) + C11H20N4OSi2 + C9H18N2O3Si2 + C7H21N3Si2 + C13H29N3OSi3 + C10H22N4OSi2 + C14H30N4O2Si3 + C8H21N5Si2 + bis(trimethylsilyl)cytosine (67014-25-9) + 7-Trimethylsilylpurin (75773-52-3) + N,N-bis(trimethysilyl)adenine (17995-04-9) + tris(trimethyl)guanine + N-Formyl-N,O-bis(trimethylsilyl)glycine (55517-31-2) + 4-(trimethylsiloxy)pyrimidine (52523-25-8) + 1,3-bis(trimethylsilyl)uracil (3442-82-8)

Guidance literature:

formamide; With ferric sulfate nonahydrate; water; at 80 ℃; for 24h;

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide; With pyridine; at 60 ℃; for 4h;

DOI:10.1002/chem.201706162

Reference yield:

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide (21149-38-2) + formamide (77287-34-4,77287-35-5,60100-09-6) → 2-methylglyoxylic acid trimethylsilyl ether (52060-85-2) + glycine trimethylsilyl ester (5269-37-4) + butanedioic acid bis(trimethylsilyl) ester (40309-57-7) + propanoic acid,2-[(trimethylsilyl)oxy] trimethylsilyl ester (17596-96-2) + [(trimethylsilyl)oxy]butanedioic acid bis(trimethylsilyl) ester (65143-63-7,107241-82-7,38166-11-9) + ethanedioic acid bis(trimethylsilyl)ester (18294-04-7) + C9H18N2O3Si2 + C7H21N3Si2 + C10H20N4Si2 + C13H29N3OSi3 + C14H30N4O2Si3 + bis(trimethylsilyl)cytosine (67014-25-9) + N,N-bis(trimethysilyl)adenine (17995-04-9) + tris(trimethyl)guanine + N-Formyl-N,O-bis(trimethylsilyl)glycine (55517-31-2) + 4-(trimethylsiloxy)pyrimidine (52523-25-8) + 1,3-bis(trimethylsilyl)uracil (3442-82-8)

Guidance literature:

formamide; With water; copper(II) nitrate; at 80 ℃; for 24h;

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide; With pyridine; at 60 ℃; for 4h;

DOI:10.1002/chem.201706162

upstream raw materials:

1,2-bis(trimethylsiloxy)cyclobutene

succinic acid

N,O-bis(trimethylsilyl)trifluoroacetamide

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide

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