Trimethylsilyl 2-[(trimethylsilyl)amino]propanoate

Base Information

• Chemical Name: Trimethylsilyl 2-[(trimethylsilyl)amino]propanoate
• CAS No.: 2899-44-7
• Molecular Formula: C9H23NO2Si2
• Molecular Weight: 233.458
• Hs Code.: 2931900090
• DSSTox Substance ID: DTXSID501248741
• Nikkaji Number: J2.847.685J
• Mol file: 2899-44-7.mol

Synonyms:N-trimethylsilylalanine trimethylsilyl ester;trimethylsilyl 2-(trimethylsilylamino)propanoate;Trimethylsilyl 2-[(trimethylsilyl)amino]propanoate;N,O-Bis-(trimethylsilyl)alanine;SCHEMBL10911927;DTXSID501248741;N-(Trimethylsilyl)alanine trimethylsilyl ester;Alanine, N-trimethylsilyl-, trimethylsilyl ester;2-[(Trimethylsilyl)amino]propanoic acid trimethylsilyl ester;2899-44-7

Chemical Property of Trimethylsilyl 2-[(trimethylsilyl)amino]propanoate

Chemical Property:

• PSA: 38.33000
• LogP: 2.56840
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 233.12673205
• Heavy Atom Count: 14
• Complexity: 206

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C(=O)O[Si](C)(C)C)N[Si](C)(C)C

Technology Process of Trimethylsilyl 2-[(trimethylsilyl)amino]propanoate

There total 3 articles about Trimethylsilyl 2-[(trimethylsilyl)amino]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide (21149-38-2) + formamide (77287-34-4,77287-35-5,60100-09-6) → N,O-bis(trimethylsilyl)-α-alanine (2899-44-7) + 2-methylglyoxylic acid trimethylsilyl ether (52060-85-2) + glycine trimethylsilyl ester (5269-37-4) + N,N'-bis(trimethylsilyl)urea (18297-63-7,127290-39-5) + butanedioic acid bis(trimethylsilyl) ester (40309-57-7) + [(trimethylsilyl)oxy]butanedioic acid bis(trimethylsilyl) ester (65143-63-7,107241-82-7,38166-11-9) + ethanedioic acid bis(trimethylsilyl)ester (18294-04-7) + C11H20N4OSi2 + C9H18N2O3Si2 + C7H21N3Si2 + C13H29N3OSi3 + C8H21N5Si2 + bis(trimethylsilyl)cytosine (67014-25-9) + 7-Trimethylsilylpurin (75773-52-3) + N,N-bis(trimethysilyl)adenine (17995-04-9) + tris(trimethyl)guanine + N-Formyl-N,O-bis(trimethylsilyl)glycine (55517-31-2) + 4-(trimethylsiloxy)pyrimidine (52523-25-8) + 1,3-bis(trimethylsilyl)uracil (3442-82-8)

Guidance literature:

formamide; With water; magnesium sulfate; at 80 ℃; for 24h;

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide; With pyridine; at 60 ℃; for 4h;

DOI:10.1002/chem.201706162

Reference yield:

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide (21149-38-2) + formamide (77287-34-4,77287-35-5,60100-09-6) → N,O-bis(trimethylsilyl)-α-alanine (2899-44-7) + glycine trimethylsilyl ester (5269-37-4) + N,N'-bis(trimethylsilyl)urea (18297-63-7,127290-39-5) + butanedioic acid bis(trimethylsilyl) ester (40309-57-7) + propanoic acid,2-[(trimethylsilyl)oxy] trimethylsilyl ester (17596-96-2) + [(trimethylsilyl)oxy]butanedioic acid bis(trimethylsilyl) ester (65143-63-7,107241-82-7,38166-11-9) + ethanedioic acid bis(trimethylsilyl)ester (18294-04-7) + C11H20N4OSi2 + C9H18N2O3Si2 + C7H21N3Si2 + C13H29N3OSi3 + C10H22N4OSi2 + C14H30N4O2Si3 + C8H21N5Si2 + bis(trimethylsilyl)cytosine (67014-25-9) + 7-Trimethylsilylpurin (75773-52-3) + N,N-bis(trimethysilyl)adenine (17995-04-9) + tris(trimethyl)guanine + N-Formyl-N,O-bis(trimethylsilyl)glycine (55517-31-2) + 4-(trimethylsiloxy)pyrimidine (52523-25-8) + 1,3-bis(trimethylsilyl)uracil (3442-82-8)

Guidance literature:

formamide; With ferric sulfate nonahydrate; water; at 80 ℃; for 24h;

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide; With pyridine; at 60 ℃; for 4h;

DOI:10.1002/chem.201706162

Reference yield:

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide (21149-38-2) + formamide (77287-34-4,77287-35-5,60100-09-6) → N,O-bis(trimethylsilyl)-α-alanine (2899-44-7) + 2-methylglyoxylic acid trimethylsilyl ether (52060-85-2) + N,N'-bis(trimethylsilyl)urea (18297-63-7,127290-39-5) + butanedioic acid bis(trimethylsilyl) ester (40309-57-7) + propanoic acid,2-[(trimethylsilyl)oxy] trimethylsilyl ester (17596-96-2) + C10H24O4Si2 (26205-45-8) + ethanedioic acid bis(trimethylsilyl)ester (18294-04-7) + C9H18N2O3Si2 + C7H21N3Si2 + C13H29N3OSi3 + C14H30N4O2Si3 + C8H21N5Si2 + 7-Trimethylsilylpurin (75773-52-3) + tris(trimethyl)guanine

Guidance literature:

formamide; With water; zinc(II) chloride; at 80 ℃; for 24h;

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide; With pyridine; at 60 ℃; for 4h;

DOI:10.1002/chem.201706162

upstream raw materials:

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide

formamide

Downstream raw materials:

DL-4-methyl-1,3-oxazolidine-2,5-dione

N-(N-Phenylaminocarbonyl)-DL-alanine

N-benzoyl-alanine trimethylsilanyl ester

N-(N-benzyloxycarbonyl-glycyl)-DL-alanine

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