Propionic acid, 2-(trimethylsiloxy)-, trimethylsilyl ester

Base Information

• Chemical Name: Propionic acid, 2-(trimethylsiloxy)-, trimethylsilyl ester
• CAS No.: 17596-96-2
• Molecular Formula: C9H22 O3 Si2
• Molecular Weight: 234.443
• Hs Code.: 2931900090
• DSSTox Substance ID: DTXSID201021853
• Nikkaji Number: J109.151D
• Mol file: 17596-96-2.mol

Synonyms:17596-96-2;Bis(trimethylsilyl)lactate;Propionic acid, 2-(trimethylsiloxy)-, trimethylsilyl ester;trimethylsilyl 2-trimethylsilyloxypropanoate;TRIMETHYLSILYL TRIMETHYLSILOXY LACTATE;Propanoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsilyl ester;Trimethylsilyl 2-[(trimethylsilyl)oxy]propanoate;o,o-Bis(trimethylsilyl)lactate;Trimethylsilyl 2-((trimethylsilyl)oxy)propanoate;Lactic acid, di-TMS;Lactic acid, bis-TMS;Lactic acid, (2TMS);Lactic acid, O,O-TMS;Lactic Acid, 2TMS derivative;DTXSID201021853;Lactic acid, bis(trimethylsilyl)oxy-, ester;2-(Trimethylsiloxy)propanoic acid trimethylsilyl ester;2-Trimethylsilyloxypropionic acid,trimethylsilyl ester;2-[(trimethylsilyl)oxy]propanoic acid trimethylsilyl ester

Chemical Property of Propionic acid, 2-(trimethylsiloxy)-, trimethylsilyl ester

Chemical Property:

• Refractive Index: 1.4053
• Boiling Point: 200°C
• PSA: 35.53000
• LogP: 2.60450
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 234.11074763
• Heavy Atom Count: 14
• Complexity: 203

Purity/Quality:

98%,99%, ^*data from raw suppliers

BIS-(TRIMETHYLSILYL)LACTATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C(=O)O[Si](C)(C)C)O[Si](C)(C)C

Technology Process of Propionic acid, 2-(trimethylsiloxy)-, trimethylsilyl ester

There total 9 articles about Propionic acid, 2-(trimethylsiloxy)-, trimethylsilyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

chloro-trimethyl-silane (75-77-4) + LACTIC ACID (849585-22-4,106989-11-1,26811-96-1,31587-11-8,26100-51-6) → propanoic acid,2-[(trimethylsilyl)oxy] trimethylsilyl ester (17596-96-2)

Guidance literature:

With 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane; at 30 ℃; for 15h;

Reference yield:

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide (21149-38-2) + formamide (77287-34-4,77287-35-5,60100-09-6) → N,O-bis(trimethylsilyl)-α-alanine (2899-44-7) + glycine trimethylsilyl ester (5269-37-4) + N,N'-bis(trimethylsilyl)urea (18297-63-7,127290-39-5) + butanedioic acid bis(trimethylsilyl) ester (40309-57-7) + propanoic acid,2-[(trimethylsilyl)oxy] trimethylsilyl ester (17596-96-2) + [(trimethylsilyl)oxy]butanedioic acid bis(trimethylsilyl) ester (65143-63-7,107241-82-7,38166-11-9) + ethanedioic acid bis(trimethylsilyl)ester (18294-04-7) + C11H20N4OSi2 + C9H18N2O3Si2 + C7H21N3Si2 + C13H29N3OSi3 + C10H22N4OSi2 + C14H30N4O2Si3 + C8H21N5Si2 + bis(trimethylsilyl)cytosine (67014-25-9) + 7-Trimethylsilylpurin (75773-52-3) + N,N-bis(trimethysilyl)adenine (17995-04-9) + tris(trimethyl)guanine + N-Formyl-N,O-bis(trimethylsilyl)glycine (55517-31-2) + 4-(trimethylsiloxy)pyrimidine (52523-25-8) + 1,3-bis(trimethylsilyl)uracil (3442-82-8)

Guidance literature:

formamide; With ferric sulfate nonahydrate; water; at 80 ℃; for 24h;

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide; With pyridine; at 60 ℃; for 4h;

DOI:10.1002/chem.201706162

Reference yield:

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide (21149-38-2) + formamide (77287-34-4,77287-35-5,60100-09-6) → 2-methylglyoxylic acid trimethylsilyl ether (52060-85-2) + glycine trimethylsilyl ester (5269-37-4) + butanedioic acid bis(trimethylsilyl) ester (40309-57-7) + propanoic acid,2-[(trimethylsilyl)oxy] trimethylsilyl ester (17596-96-2) + [(trimethylsilyl)oxy]butanedioic acid bis(trimethylsilyl) ester (65143-63-7,107241-82-7,38166-11-9) + ethanedioic acid bis(trimethylsilyl)ester (18294-04-7) + C9H18N2O3Si2 + C7H21N3Si2 + C10H20N4Si2 + C13H29N3OSi3 + C14H30N4O2Si3 + bis(trimethylsilyl)cytosine (67014-25-9) + N,N-bis(trimethysilyl)adenine (17995-04-9) + tris(trimethyl)guanine + N-Formyl-N,O-bis(trimethylsilyl)glycine (55517-31-2) + 4-(trimethylsiloxy)pyrimidine (52523-25-8) + 1,3-bis(trimethylsilyl)uracil (3442-82-8)

Guidance literature:

formamide; With water; copper(II) nitrate; at 80 ℃; for 24h;

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide; With pyridine; at 60 ℃; for 4h;

DOI:10.1002/chem.201706162

upstream raw materials:

chloro-trimethyl-silane

LACTIC ACID

N,O-bis(trimethylsilyl)trifluoroacetamide

2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide

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