2,3-Dihydro-7-hydroxy-3-methyl-1H-inden-1-one

Base Information

• Chemical Name: 2,3-Dihydro-7-hydroxy-3-methyl-1H-inden-1-one
• CAS No.: 40513-50-6
• Molecular Formula: C10H10O2
• Molecular Weight: 162.18500
• Mol file: 40513-50-6.mol

Synonyms:7-Hydroxy-3-methyl-1-indanon;7-Hydroxy-3-methylindanon-(1);3-Methyl-7-hydroxy-1-indanon;7-hydroxy-3-methyl-indan-1-one;7-Hydroxy-3-methyl-1-indanone;7-Hydroxy-3-methyl-indan-1-on;

Chemical Property of 2,3-Dihydro-7-hydroxy-3-methyl-1H-inden-1-one

Chemical Property:

• Boiling Point: 85 °C (0.3 mmHg)
• PSA: 37.30000
• LogP: 2.08210

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-Dihydro-7-hydroxy-3-methyl-1H-inden-1-one

There total 7 articles about 2,3-Dihydro-7-hydroxy-3-methyl-1H-inden-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

4-butanolide (96-48-0) + phenol (108-95-2,27073-41-2) → 7-hydroxy-3-methylindan-1-one (40513-50-6)

Guidance literature:

With aluminum (III) chloride; sodium chloride; at 180 ℃; for 2h;

DOI:10.1002/anie.202110009

Reference yield: 14.0%

4-bromo-7-hydroxy-3-methylindanone (104517-25-1) → 7-hydroxy-3-methylindan-1-one (40513-50-6)

Guidance literature:

With aluminium trichloride; 1) 145 deg C, 4 h, 2) 160 deg C, 1 h.;

Reference yield:

ethyl-alpha-bromophenyl acetate (6308-89-0) → 7-hydroxy-3-methylindan-1-one (40513-50-6)

Guidance literature:

With aluminium trichloride;

DOI:10.1021/ja01112a042

upstream raw materials:

4-butanolide

ethyl-alpha-bromophenyl acetate

phenol

4-bromo-7-hydroxy-3-methylindanone

Downstream raw materials:

7-hydroxy-3-methylindan-1-(N-2,6-diisopropylphenylimine)

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