4-METHYL-2H-[1,2,4]TRIAZINE-3,5-DIONE

Base Information

• Chemical Name: 4-METHYL-2H-[1,2,4]TRIAZINE-3,5-DIONE
• CAS No.: 1627-30-1
• Molecular Formula: C4H5 N3 O2
• Molecular Weight: 127.1014
• Hs Code.: 2933699090
• Mol file: 1627-30-1.mol

Synonyms:as-Triazine-3,5(2H,4H)-dione,4-methyl- (6CI,7CI,8CI); 3-Methyl-6-azauracil;4-Methyl-3,5-dioxo-2H,4H-1,2,4-triazine; 6-Aza-3-methyluracil; NSC 227398; NSC58979

Chemical Property of 4-METHYL-2H-[1,2,4]TRIAZINE-3,5-DIONE

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 67.75000
• Density: 1.54g/cm³
• LogP: -1.53140

Purity/Quality:

97% ^*data from raw suppliers

4-Methyl-1,2,4-triazine-3,5(2H,4H)-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-METHYL-2H-[1,2,4]TRIAZINE-3,5-DIONE

There total 4 articles about 4-METHYL-2H-[1,2,4]TRIAZINE-3,5-DIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.3%

2-acetyl-4-methyl-1,2,4-triazine-3,5(2H,4H)-dione (88512-99-6) → 4-methyl-1,2,4-triazine-3,5(2H,4H)-dione (1627-30-1)

Guidance literature:

With toluene-4-sulfonic acid; In ethanol; at 60 ℃;

DOI:10.1007/s11696-019-00685-1

Reference yield:

toluene-4-sulfonic acid (104-15-4) + 2-acetyl-2H,3H,4H,5H-[1,2,4]-triazin-3,5-dione (4338-50-5) → 4-methyl-1,2,4-triazine-3,5(2H,4H)-dione (1627-30-1)

Guidance literature:

With CH₃I; NaH; In ethanol; water; N,N-dimethyl-formamide; paraffin;

Reference yield:

2-acetyl-2H,3H,4H,5H-[1,2,4]-triazin-3,5-dione (4338-50-5) + methyl iodide (74-88-4) → 4-methyl-1,2,4-triazine-3,5(2H,4H)-dione (1627-30-1)

Guidance literature:

In ethanol; water; N,N-dimethyl-formamide;

upstream raw materials:

2-acetyl-4-methyl-1,2,4-triazine-3,5(2H,4H)-dione

2-acetyl-2H,3H,4H,5H-[1,2,4]-triazin-3,5-dione

methyl iodide

toluene-4-sulfonic acid

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