3(2H)-Oxazoleacetic acid, a-(hydroxymethyl)-2-oxo-4,5-diphenyl-, (S)-, compd. with N-cyclohexylcyclohexanamine (1:1)

Base Information

Chemical Name:3(2H)-Oxazoleacetic acid, a-(hydroxymethyl)-2-oxo-4,5-diphenyl-, (S)-, compd. with N-cyclohexylcyclohexanamine (1:1)
CAS No.:40719-42-4
Molecular Formula:C18H15NO5.C12H23N
Molecular Weight:506.642
Hs Code.:
Mol file:40719-42-4.mol

Synonyms:

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Chemical Property of 3(2H)-Oxazoleacetic acid, a-(hydroxymethyl)-2-oxo-4,5-diphenyl-, (S)-, compd. with N-cyclohexylcyclohexanamine (1:1)

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Technology Process of 3(2H)-Oxazoleacetic acid, a-(hydroxymethyl)-2-oxo-4,5-diphenyl-, (S)-, compd. with N-cyclohexylcyclohexanamine (1:1)

There total 1 articles about 3(2H)-Oxazoleacetic acid, a-(hydroxymethyl)-2-oxo-4,5-diphenyl-, (S)-, compd. with N-cyclohexylcyclohexanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21240-34-6
4,5-diphenyl-1,3-dioxol-2-one

: 56-45-1,83245-15-2
L-serin

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 40719-42-4
L-Ox-serine dicyclohexylammonium salt

Guidance literature:: Multistep reaction; (i) OH, MeOH, (ii) /BRN= 1114120/, DMF, (iii) CF3CO2H, (iv) /BRN= 605923/, EtOH, Et2O;
DOI:10.1021/jo00957a024

Reference yield: 71.0%

: 1443793-28-9
L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate

: 40719-42-4
L-Ox-serine dicyclohexylammonium salt

: 1443793-29-0
N-(4,6-diphenyl-4-oxazolin-2-onyl)-L-seryl-L-[p-(benzyloxy)phenyl]glycine tert-butyl ester

Guidance literature:: L-Ox-serine dicyclohexylammonium salt; With (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.0166667h;

L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;
DOI:10.1021/jo4007893

Reference yield: 69.0%

: 123004-72-8
D-glycine tert-butyl ester toluenesulfonate salt

: 40719-42-4
L-Ox-serine dicyclohexylammonium salt

: 110207-46-0
(-)-3-N-(4,5-diphenyl-4-oxazolin-2-onyl)aminocardicinic acid tert-butyl ester

Guidance literature:: L-Ox-serine dicyclohexylammonium salt; With (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.0166667h;

D-glycine tert-butyl ester toluenesulfonate salt; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;
DOI:10.1021/jo4007893