L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate

Base Information

Chemical Name:L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate
CAS No.:1443793-28-9
Molecular Formula:C₇H₈O₃S*C₁₉H₂₃NO₃
Molecular Weight:485.601
Hs Code.:

Synonyms:L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate

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Chemical Property of L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate

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Technology Process of L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate

There total 1 articles about L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 104-15-4
toluene-4-sulfonic acid

: 115-11-7,15220-85-6
isobutene

: 336877-72-6
L-2-[p-(benzyloxy)phenyl]glycine

: 1443793-28-9
L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate

Guidance literature:: With sulfuric acid; In 1,4-dioxane; diethyl ether;
DOI:10.1021/jo4007893

Reference yield: 71.0%

: 1443793-28-9
L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate

: 40719-42-4
L-Ox-serine dicyclohexylammonium salt

: 1443793-29-0
N-(4,6-diphenyl-4-oxazolin-2-onyl)-L-seryl-L-[p-(benzyloxy)phenyl]glycine tert-butyl ester

Guidance literature:: L-Ox-serine dicyclohexylammonium salt; With (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.0166667h;

L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;
DOI:10.1021/jo4007893

Reference yield:

: 1443793-28-9
L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate

: 1443793-30-3
3-N-(4,5-diphenyl-4-oxazolin-2-onyl)-epi-aminonocardicin tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0.02 h / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: diethylazodicarboxylate; triethyl phosphite / tetrahydrofuran / 12 h / 20 °C / Darkness

With (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; diethylazodicarboxylate; triethyl phosphite; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo4007893