Propanoic acid, 2-methyl-, phenylmethylene ester

Base Information

• Chemical Name: Propanoic acid, 2-methyl-, phenylmethylene ester
• CAS No.: 413601-57-7
• Molecular Formula: C15H20O4
• Molecular Weight: 264.321
• Mol file: 413601-57-7.mol

Synonyms:

Chemical Property of Propanoic acid, 2-methyl-, phenylmethylene ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Propanoic acid, 2-methyl-, phenylmethylene ester

There total 1 articles about Propanoic acid, 2-methyl-, phenylmethylene ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-Methylpropionic anhydride (97-72-3) + benzaldehyde (100-52-7) → bis(2-methylpropanoyloxy)phenylmethane (413601-57-7)

Guidance literature:

With tetra-N-butylammonium tribromide; at 20 ℃; for 4h;

DOI:10.1002/ejoc.200400584

Reference yield: 97.0%

bis(2-methylpropanoyloxy)phenylmethane (413601-57-7) → benzaldehyde (100-52-7)

Guidance literature:

With tetra-N-butylammonium tribromide; In methanol; at 20 ℃; for 0.75h;

DOI:10.1002/ejoc.200400584

Reference yield:

bis(2-methylpropanoyloxy)phenylmethane (413601-57-7) → benzyl 2-methylpropanoate (103-28-6)

Guidance literature:

With zinc; In acetonitrile; at 70 ℃; for 24h;

DOI:10.1016/j.tet.2003.10.068

upstream raw materials:

2-Methylpropionic anhydride

benzaldehyde

Downstream raw materials:

benzyl 2-methylpropanoate

benzaldehyde

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