N~1~,N~1~,N~2~,N~2~-tetramethyl-4-cyclohexene-1,2-dicarboxamide

Base Information

• Chemical Name: N~1~,N~1~,N~2~,N~2~-tetramethyl-4-cyclohexene-1,2-dicarboxamide
• CAS No.: 39214-27-2
• Molecular Formula: C12H20N2O2
• Molecular Weight: 224.3
• NSC Number: 121491
• DSSTox Substance ID: DTXSID60959989
• Mol file: 39214-27-2.mol

Synonyms:39214-27-2;N~1~,N~1~,N~2~,N~2~-tetramethyl-4-cyclohexene-1,2-dicarboxamide;1-N,1-N,2-N,2-N-tetramethylcyclohex-4-ene-1,2-dicarboxamide;NSC121491;DTXSID60959989;NSC-121491;AD-266/41884742;N~1~,N~1~,N~2~,N~2~-Tetramethylcyclohex-4-ene-1,2-dicarboxamide

Chemical Property of N~1~,N~1~,N~2~,N~2~-tetramethyl-4-cyclohexene-1,2-dicarboxamide

Chemical Property:

• Boiling Point: 377.1oC at 760 mmHg
• Flash Point: 164.4oC
• PSA: 40.62000
• Density: 1.069g/cm3
• LogP: 0.74520
• XLogP3: 0.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 224.152477885
• Heavy Atom Count: 16
• Complexity: 278

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C(=O)C1CC=CCC1C(=O)N(C)C

Technology Process of N~1~,N~1~,N~2~,N~2~-tetramethyl-4-cyclohexene-1,2-dicarboxamide

There total 3 articles about N~1~,N~1~,N~2~,N~2~-tetramethyl-4-cyclohexene-1,2-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl amine (124-40-3) → (+/-)-tetra-N-methyl-trans-cyclohex-4-ene-1,2-dicarboxamide (39214-27-2,70179-67-8)

Guidance literature:

DOI:10.1021/ja01651a040

Reference yield:

N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) + 1,2,3,6-Tetrahydrophthalic anhydride (85-43-8) → 1,2,3,6-Tetrahydrophthalsaeure-bis-dimethylamid (39214-27-2)

Guidance literature:

at 180 - 240 ℃;

Reference yield:

→ Δ4-Cyclohexen-trans-bis- (39214-27-2,70179-67-8)

Guidance literature:

1,3-Butadien, 1. Fumaroylchlorid -> entspr. Diels-Alder-Addukt, 2. Dimethylamin;

DOI:10.1016/S0040-4039(01)87505-5

upstream raw materials:

N,N,N,N,N,N-hexamethylphosphoric triamide

1,2,3,6-Tetrahydrophthalic anhydride

dimethyl amine

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