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124-40-3

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Product FOB Price Min.Order Supply Ability Supplier
Dimethylamine solution, 40 wt. % in water 124-40-3
Cas No: 124-40-3
No Data No Data No Data Hunan Russell Chemicals Technology Co.,Ltd Contact Supplier
Dimethylamine
Cas No: 124-40-3
No Data 100 Kilogram 20 Metric Ton/Month Jiangxi Sunway Chemical Co. Ltd. Contact Supplier

124-40-3 Usage

Fire Hazard

FLAMMABLE. Flashback along vapor trail may occur. May explode if ignited in an enclosed area. Vapors are eye, skin and respiratory irritants.

Health Hazard

VAPOR: Irritating to eyes, nose and throat. If inhaled, will cause difficult breathing. LIQUID. Will burn skin and eyes. Harmful if swallowed.

Purification Methods

Dry dimethylamine by passage through a KOH-filled tower, or by standing with sodium pellets at 0o during 18hours. [Beilstein 4 IV 128.]

Reactivity Profile

DIMETHYLAMINE is a base, neutralizing acids in exothermic reactions, and a reducing agent. Dimethylamine is temperature sensitive. Reacts vigorously with mercury and chlorine . Reacts violently with strong oxidizing agents and attacks copper and copper compounds [Handling Chemicals Safely, 1980 p. 123]. Reacts with hypochlorites to give N-chloroamines, some of which are explosives when isolated [Bretherick, 1979 p. 108].

Air & Water Reactions

Highly flammable. Water soluble.

Chemical Properties

colourless gas with strong ammonia-like smell

General Description

A colorless gas smelling of fish at low concentrations and of ammonia at higher concentrations. Shipped as a liquid under its vapor pressure. Contact with the unconfined liquid can cause frostbite by evaporative cooling and chemical type burns. Density of liquid 5.5 lb / gal. The gas, which is corrosive, dissolves readily in water to form flammable corrosive solutions. The gas is heavier than air and can asphyxiate by the displacement of air. Gas is easily ignited and produces toxic oxides of nitrogen when burned. Long-term inhalation of low concentrations or short-term inhalation of low concentrations has adverse health effects. Under prolonged exposure to fire or intense heat the containers may rupture violently and rocket. Used to make other chemicals and as a solvent.

Description

Dimethylamine is a colourless flammable gas at room temperature. It has a pungent, fishy, or ammonia-like odour at room temperature and is shipped and marketed in compressed liquid form. It is very soluble in water and soluble in alcohol and ether. It is incompatible with oxidising materials, acrylaldehyde, fluorine, maleic anhydride, chlorine, or mercury. Dimethylamine is a precursor to several industrially important compounds. For instance, it used in the manufacture of several products, for example, for the vulcanisation process of rubber, as detergent soaps, in leather tanning, in the manufacture of pharmaceuticals, and also for cellulose acetate rayon treatment.

Definition

ChEBI: A secondary aliphatic amine where both N-substituents are methyl.
InChI:InChI=1/C2H7N/c1-3-2;1-5(2,3)4/h3H,1-2H3;(H2,1,2,3,4)/p-2

124-40-3 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (43261)  Dimethylamine, 40% w/w aq. soln.    124-40-3 50each 829.0CNY Detail
Alfa Aesar (43261)  Dimethylamine, 40% w/w aq. soln.    124-40-3 10each 298.0CNY Detail
Alfa Aesar (31458)  Dimethylamine, 40% w/w aq. soln.    124-40-3 3kg 424.0CNY Detail
Alfa Aesar (31458)  Dimethylamine, 40% w/w aq. soln.    124-40-3 1kg 178.0CNY Detail
Alfa Aesar (31458)  Dimethylamine, 40% w/w aq. soln.    124-40-3 250g 68.0CNY Detail
Alfa Aesar (H27665)  Dimethylamine, 2M in THF    124-40-3 1000ml 3636.0CNY Detail
Alfa Aesar (H27665)  Dimethylamine, 2M in THF    124-40-3 100ml 601.0CNY Detail
Alfa Aesar (H27261)  Dimethylamine, 2M in methanol    124-40-3 100ml 842.0CNY Detail
Alfa Aesar (H27261)  Dimethylamine, 2M in methanol    124-40-3 25ml 515.0CNY Detail

124-40-3SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Dimethylamine

1.2 Other means of identification

Product number -
Other names N-methylmethanamine

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Agricultural chemicals (non-pesticidal),Intermediates,Ion exchange agents,Lubricants and lubricant additives,Paint additives and coating additives not described by other categories
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:124-40-3 SDS

124-40-3Synthetic route

N-Nitrosodimethylamine
62-75-9

N-Nitrosodimethylamine

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With iron; nickel In water pH=6.3 - 9.2; Kinetics; Further Variations:; Reagents; Hydrogenation;100%
With isocyanate de chlorosulfonyle In diethyl ether for 10h; Ambient temperature;65%
With titanium(III) chloride; water
3-ethynyl-cyclohepta-1.3.5-triene
85809-41-2

3-ethynyl-cyclohepta-1.3.5-triene

(dimethylamino)trimethyltin
993-50-0

(dimethylamino)trimethyltin

A

3-(trimethylstannylethynyl)-1,3,5-cycloheptatriene
286387-63-1

3-(trimethylstannylethynyl)-1,3,5-cycloheptatriene

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
In neat (no solvent) Me3SnNMe2 added to 3-ethynyl-1,3,5-cycloheptatriene, react. mixture stirred without a solvent for 5 min at ambient temp., Me2NH evapd.; Me2NH evapd., product isolated in quant. yield;A 100%
B n/a
N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

benzylamine
100-46-9

benzylamine

A

N-benzylformamide
6343-54-0

N-benzylformamide

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With 2,3-dihydrophthalazine-1,4-dione at 80 - 95℃; for 40h;A 99%
B n/a
With cerium(IV) oxide at 100℃; for 12h; Reagent/catalyst;
C13H23N3O3S

C13H23N3O3S

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

C15H23N3O5S

C15H23N3O5S

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With 2,3-dihydrophthalazine-1,4-dione at 80 - 95℃; for 40h;A 98%
B n/a
1-dimethylamino-2,4-dinitronaphthalene
39139-79-2

1-dimethylamino-2,4-dinitronaphthalene

ethylamine
75-04-7

ethylamine

A

N-ethyl-2,4-dinitro-1-naphthylamine
27210-67-9

N-ethyl-2,4-dinitro-1-naphthylamine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
In water at 30℃; for 2h;A 98%
B n/a
propylamine
107-10-8

propylamine

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester
71240-22-7

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-(1H-Benzoimidazol-2-yl)-3-propylamino-acrylic acid ethyl ester

(E)-2-(1H-Benzoimidazol-2-yl)-3-propylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 40℃; for 0.5h; Irradiation;A n/a
B 98%
SEC-BUTYLAMINE
33966-50-6

SEC-BUTYLAMINE

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester
71240-22-7

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-(1H-Benzoimidazol-2-yl)-3-sec-butylamino-acrylic acid ethyl ester

(E)-2-(1H-Benzoimidazol-2-yl)-3-sec-butylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 60℃; for 0.5h; Irradiation;A n/a
B 98%
N,N-dimethylammonium chloride
506-59-2

N,N-dimethylammonium chloride

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With potassium hydroxide In water Inert atmosphere;98%
With potassium hydroxide In dichloromethane at -15 - -5℃; for 1h;90%
With potassium hydroxide Alkaline conditions;
N',N''-dicyclohexyl-N,N-dimethylguanidine
29882-02-8

N',N''-dicyclohexyl-N,N-dimethylguanidine

cyclohexylamine
108-91-8

cyclohexylamine

A

N,N',N''-tricyclohexylguanidine
4833-41-4

N,N',N''-tricyclohexylguanidine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 98%
B n/a
2-benzooxazol-2-yl-3-dimethylamino-acrylic acid ethyl ester
71240-24-9

2-benzooxazol-2-yl-3-dimethylamino-acrylic acid ethyl ester

tert-butylamine
75-64-9

tert-butylamine

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-Benzooxazol-2-yl-3-tert-butylamino-acrylic acid ethyl ester

(E)-2-Benzooxazol-2-yl-3-tert-butylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 40℃; for 0.5h; Irradiation;A n/a
B 97%
tert-butylamine
75-64-9

tert-butylamine

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester
71240-22-7

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-(1H-Benzoimidazol-2-yl)-3-tert-butylamino-acrylic acid ethyl ester

(E)-2-(1H-Benzoimidazol-2-yl)-3-tert-butylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 40℃; for 0.5h; Irradiation;A n/a
B 97%
o-chloranil
1198-55-6

o-chloranil

Hexamethylphosphorous triamide
1608-26-0

Hexamethylphosphorous triamide

A

dimethyl amine
124-40-3

dimethyl amine

B

tetrachlorobenzo<1,3,2>dioxaphosphol-2-yl-dimethylamine
320747-63-5

tetrachlorobenzo<1,3,2>dioxaphosphol-2-yl-dimethylamine

Conditions
ConditionsYield
With ammonium chloride In toluene for 1.5h; Heating;A n/a
B 97%
pyrrolidine
123-75-1

pyrrolidine

N',N''-dicyclohexyl-N,N-dimethylguanidine
29882-02-8

N',N''-dicyclohexyl-N,N-dimethylguanidine

A

N,N'-dicyclohexylpyrrolidine-1-carboximidamide
60006-28-2

N,N'-dicyclohexylpyrrolidine-1-carboximidamide

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 97%
B n/a
N',N''-dicyclohexyl-N,N-dimethylguanidine
29882-02-8

N',N''-dicyclohexyl-N,N-dimethylguanidine

isopropylamine
75-31-0

isopropylamine

A

N,N'-Dicyclohexyl-N''-isopropyl-guanidin

N,N'-Dicyclohexyl-N''-isopropyl-guanidin

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 97%
B n/a
tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

3-Dimethylamino-2-(formylaminomethyl)acrylsaeure-ethylester
74119-34-9

3-Dimethylamino-2-(formylaminomethyl)acrylsaeure-ethylester

A

ethyl 3-(dimethylamino)acrylate
924-99-2, 1117-37-9, 114894-59-6

ethyl 3-(dimethylamino)acrylate

B

dimethyl amine
124-40-3

dimethyl amine

C

tert-butyl alcohol
75-65-0

tert-butyl alcohol

Conditions
ConditionsYield
at 160℃; for 3h;A 96%
B n/a
C n/a
piperidine
110-89-4

piperidine

N',N''-dicyclohexyl-N,N-dimethylguanidine
29882-02-8

N',N''-dicyclohexyl-N,N-dimethylguanidine

A

N,N'-dicyclohexylpiperidine-1-carboximidamide
60006-25-9

N,N'-dicyclohexylpiperidine-1-carboximidamide

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 96%
B n/a
N,N-dimethylhexa-1,5-dien-3-amine
75712-80-0

N,N-dimethylhexa-1,5-dien-3-amine

A

hex-5-en-1-al
764-59-0

hex-5-en-1-al

B

(E)-N,N-Dimethyl-1,5-hexadien-1-amin
82574-98-9

(E)-N,N-Dimethyl-1,5-hexadien-1-amin

C

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
at 223.5℃; for 12h;A n/a
B 95.8%
C n/a
at 160.2 - 200.1℃; Yield given. Yields of byproduct given;
With N,N-dimethyl-cyclohexanamine at 160.2 - 200.1℃; under 3 Torr; Kinetics; Thermodynamic data; Cope rearrengament, ΔH*, ΔG*, ΔS*, Ea;
((CH3)2N)2PH(Fe(CO)4)
116018-88-3

((CH3)2N)2PH(Fe(CO)4)

(PPh4)(hydridoiron(carbonyl)4)
103616-27-9

(PPh4)(hydridoiron(carbonyl)4)

A

((CH3)2N)PH(Fe(CO)4)2(1-)*(C6H5)4P(1+)={(C6H5)4P}{(CH3)2NPH(Fe(CO)4)2}

((CH3)2N)PH(Fe(CO)4)2(1-)*(C6H5)4P(1+)={(C6H5)4P}{(CH3)2NPH(Fe(CO)4)2}

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
A 95%
B n/a
3-(Dimethylaminomethyl)indole
87-52-5

3-(Dimethylaminomethyl)indole

ethylamine
75-04-7

ethylamine

A

3-(N-ethylamino)methylindole
57506-90-8

3-(N-ethylamino)methylindole

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
Heating;A 94%
B n/a
isopropylamine
75-31-0

isopropylamine

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester
71240-22-7

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-(1H-Benzoimidazol-2-yl)-3-isopropylamino-acrylic acid ethyl ester

(E)-2-(1H-Benzoimidazol-2-yl)-3-isopropylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 30℃; for 0.5h; Irradiation;A n/a
B 94%
isopropylamine
75-31-0

isopropylamine

N′,N″-diisopropyl-N,N-dimethyl guanidine
68897-42-7

N′,N″-diisopropyl-N,N-dimethyl guanidine

A

N,N', N''-tri(isopropyl)guanidine
121948-77-4

N,N', N''-tri(isopropyl)guanidine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 94%
B n/a
N-(N3-p-toluenesulfonyl)-3-aminopropylphthalimide
38353-77-4

N-(N3-p-toluenesulfonyl)-3-aminopropylphthalimide

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

2,3-dihydrophthalazine-1,4-dione
1445-69-8

2,3-dihydrophthalazine-1,4-dione

B

N1-formyl-N3-tosyl-1,3-propanediamine
107976-50-1

N1-formyl-N3-tosyl-1,3-propanediamine

C

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With hydrazine hydrate at 80℃; for 3h;A n/a
B 93%
C n/a
ethyl (2E/Z)-2-(1,3-benzothiazol-2-yl)-3-(dimethylamino)acrylate
71240-23-8

ethyl (2E/Z)-2-(1,3-benzothiazol-2-yl)-3-(dimethylamino)acrylate

propylamine
107-10-8

propylamine

A

dimethyl amine
124-40-3

dimethyl amine

B

(Z)-2-Benzothiazol-2-yl-3-propylamino-acrylic acid ethyl ester

(Z)-2-Benzothiazol-2-yl-3-propylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 40℃; for 0.5h; Irradiation;A n/a
B 93%
tetrakis(dimethylamido)diborane
1630-79-1

tetrakis(dimethylamido)diborane

N-butylamine
109-73-9

N-butylamine

A

tetrakis(n-butylamino)diborane(4)
7360-73-8

tetrakis(n-butylamino)diborane(4)

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
In hexane heating from 76 to 174°C during 21.6 h;A 93%
B n/a
4 equiv. n-C4H9NH2, slow react. at room temp.;
4 equiv. n-C4H9NH2, slow react. at room temp.;
(2-bromoethyl)dimethyl-(3,3-dimethylallyl)ammonium bromide
58369-78-1

(2-bromoethyl)dimethyl-(3,3-dimethylallyl)ammonium bromide

1-amino-2-propene
107-11-9

1-amino-2-propene

A

Allyl-[3,3-dimethyl-pent-4-en-(E)-ylidene]-amine
88019-80-1

Allyl-[3,3-dimethyl-pent-4-en-(E)-ylidene]-amine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With potassium hydroxide In water at 90 - 95℃; for 1h;A 92.7%
B 79.5%
With potassium hydroxide In water at 90 - 95℃; for 1h; Product distribution; ratio of reactants;A 92.7%
B 79.5%
cyclohexylamine
108-91-8

cyclohexylamine

N′,N″-diisopropyl-N,N-dimethyl guanidine
68897-42-7

N′,N″-diisopropyl-N,N-dimethyl guanidine

A

dimethyl amine
124-40-3

dimethyl amine

B

2-Cyclohexyl-1,3-diisopropylguanidine

2-Cyclohexyl-1,3-diisopropylguanidine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A n/a
B 92%
3-(Dimethylaminomethyl)indole
87-52-5

3-(Dimethylaminomethyl)indole

cyclohexylamine
108-91-8

cyclohexylamine

A

N-indol-3-ylmethylcyclohexylamine
53924-03-1

N-indol-3-ylmethylcyclohexylamine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
Heating;A 91%
B n/a
Conditions
ConditionsYield
With water at 25℃; Product distribution; Mechanism; anodic oxidation, carbonate buffer, pH 10; effect of substituents investigated with different types of β-alkanolamines;A 6.4%
B 0.5%
C 91%
D 90%
E 91%
1,1-dimethylhydrazine
57-14-7

1,1-dimethylhydrazine

β-naphthol
135-19-3

β-naphthol

A

1-amino-2-naphthol
2834-92-6

1-amino-2-naphthol

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
at 80℃; for 4h;A 91%
B n/a
(2-bromoethyl)dimethyl-(3,3-dimethylallyl)ammonium bromide
58369-78-1

(2-bromoethyl)dimethyl-(3,3-dimethylallyl)ammonium bromide

aniline
62-53-3

aniline

A

[3,3-Dimethyl-pent-4-en-(E)-ylidene]-phenyl-amine
88019-86-7

[3,3-Dimethyl-pent-4-en-(E)-ylidene]-phenyl-amine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With potassium hydroxide In water at 90 - 95℃; for 1h;A 90.9%
B 84.9%
2-methyl-1,2-epoxypropane
558-30-5

2-methyl-1,2-epoxypropane

dimethyl amine
124-40-3

dimethyl amine

1-dimethylamino-2-methyl-propan-2-ol
14123-48-9

1-dimethylamino-2-methyl-propan-2-ol

Conditions
ConditionsYield
In water at -5 - 20℃; Schlenk technique; Inert atmosphere; Sealed tube;100%
With water In water at 20 - 50℃; for 120h; Sealed tube;91%
In water at 20℃; for 12h; Cooling with ice; Inert atmosphere;89%
2-chloropyridine-5-sulfonyl chloride
6684-39-5

2-chloropyridine-5-sulfonyl chloride

dimethyl amine
124-40-3

dimethyl amine

6-chloro-N,N-dimethylpyridine-3-sulfonamide
52480-31-6

6-chloro-N,N-dimethylpyridine-3-sulfonamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 2h;100%
With triethylamine In tetrahydrofuran at 20℃; for 0.5h;95%
With triethylamine In tetrahydrofuran at 20℃; for 0.5h;95%
1,10-dibromodecane
4101-68-2

1,10-dibromodecane

dimethyl amine
124-40-3

dimethyl amine

N,N,N',N'-tetramethyl-1,10-diaminodecane
1938-62-1

N,N,N',N'-tetramethyl-1,10-diaminodecane

Conditions
ConditionsYield
In chloroform at 20℃; for 24h;100%
With sodium carbonate In ethanol; water for 24h; Heating;92%
With ethanol
In benzene at 4 - 5℃;
at 4 - 5℃;
succinoyl dichloride
543-20-4

succinoyl dichloride

dimethyl amine
124-40-3

dimethyl amine

N,N,N',N'-tetramethylsuccinamide
7334-51-2

N,N,N',N'-tetramethylsuccinamide

Conditions
ConditionsYield
In water at 0℃; for 0.5h;100%
In diethyl ether at -78 - 20℃;91%
In dichloromethane; water at 0 - 20℃; for 20h; Inert atmosphere;81%
With diethyl ether
In water at 0℃; for 0.5h;
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

dimethyl amine
124-40-3

dimethyl amine

N,N,N',N'-tetramethylhexamethylenediamine
111-18-2

N,N,N',N'-tetramethylhexamethylenediamine

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 20℃; for 24h;100%
In chloroform at 20℃; for 24h;100%
With sodium carbonate In ethanol; water for 24h; Heating;98%
cholic acid
81-25-4

cholic acid

dimethyl amine
124-40-3

dimethyl amine

(R)-N,N-dimethyl-4-((3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-3,7,12-trihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthrene-17-yl)valeramide
86678-85-5

(R)-N,N-dimethyl-4-((3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-3,7,12-trihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthrene-17-yl)valeramide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere;100%
With tributyl-amine; chloroformic acid ethyl ester In 1,4-dioxane 10 deg C, 30 min then rt., 2 h;78%
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 10h;74.2%
With water at 250℃;
With tributyl-amine; chloroformic acid ethyl ester Multistep reaction;
dimethyl amine
124-40-3

dimethyl amine

ethylene dibromide
106-93-4

ethylene dibromide

N,N,N,N,-tetramethylethylenediamine
110-18-9

N,N,N,N,-tetramethylethylenediamine

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 20℃; for 24h;100%
In chloroform at 20℃; for 24h;100%
dimethyl amine
124-40-3

dimethyl amine

propynoic acid methyl ester
922-67-8

propynoic acid methyl ester

methyl 3-(N,N-dimethylamino)-2-propenoate
999-59-7

methyl 3-(N,N-dimethylamino)-2-propenoate

Conditions
ConditionsYield
In diethyl ether at 20℃; for 1h;100%
With benzene
dimethyl amine
124-40-3

dimethyl amine

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

N,N,4-trimethylbenzenesulfonamide
599-69-9

N,N,4-trimethylbenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 25℃; for 1h;100%
99%
With cesium fluoride supported on Celite at 50℃; for 0.75h; chemoselective reaction;91%
dimethyl amine
124-40-3

dimethyl amine

N-Nitrosodimethylamine
62-75-9

N-Nitrosodimethylamine

Conditions
ConditionsYield
With sulfuric acid; silica gel; sodium nitrite In dichloromethane at 20℃; for 0.5h; Nitrosation;100%
With Nafion-H(R); silica gel; sodium nitrite In dichloromethane at 20℃; for 0.166667h;100%
With trichloromelamine; silica gel; sodium nitrite In dichloromethane; water at 20℃; for 0.0333333h;100%
2-chloro-1,3-benzoxazole
615-18-9

2-chloro-1,3-benzoxazole

dimethyl amine
124-40-3

dimethyl amine

2-dimethylaminobenzoxazole
13858-89-4

2-dimethylaminobenzoxazole

Conditions
ConditionsYield
In tetrahydrofuran; water for 0.166667h; Inert atmosphere; Reflux;100%
In water at 20℃; for 1h;90%
In water at 20℃; for 5h; Green chemistry;71%
benzonitrile
100-47-0

benzonitrile

dimethyl amine
124-40-3

dimethyl amine

N,N-Dimethyl-benzamidine
20548-18-9, 39116-58-0

N,N-Dimethyl-benzamidine

Conditions
ConditionsYield
Stage #1: dimethyl amine With n-butyllithium In diethyl ether; hexane at -20℃; for 0.166667h;
Stage #2: benzonitrile at -20℃; for 1h;
100%
phenylborondichloride
873-51-8

phenylborondichloride

dimethyl amine
124-40-3

dimethyl amine

Bis-(dimethylamino)-phenylboran
1201-45-2

Bis-(dimethylamino)-phenylboran

Conditions
ConditionsYield
In pentane at -78 - 20℃; Inert atmosphere;100%
In hexane87%
In hexane87%
1 ,4-phenylenediisothiocyanate
4044-65-9

1 ,4-phenylenediisothiocyanate

dimethyl amine
124-40-3

dimethyl amine

3-[4-(3,3-dimethyl-thioureido)-phenyl]-1,1-dimethyl-thiourea
16349-56-7

3-[4-(3,3-dimethyl-thioureido)-phenyl]-1,1-dimethyl-thiourea

Conditions
ConditionsYield
at 20℃; under 750.06 Torr; Addition; solid-gas reaction;100%
dimethyl amine
124-40-3

dimethyl amine

Cinnamoyl chloride
102-92-1

Cinnamoyl chloride

(E)-N,N-dimethylcinnamamide
17431-39-9

(E)-N,N-dimethylcinnamamide

Conditions
ConditionsYield
In water at 0℃; for 0.75h;100%
In methanol for 15h; Ambient temperature;81%
In diethyl ether for 0.5h;46.9%
dimethyl amine
124-40-3

dimethyl amine

NBD chloride
10199-89-0

NBD chloride

N,N-dimethyl-7-nitrobenzo[c][1,2,5]oxadiazol-4-amine
1455-87-4

N,N-dimethyl-7-nitrobenzo[c][1,2,5]oxadiazol-4-amine

Conditions
ConditionsYield
In methanol100%
In dichloromethane at 20℃; for 2h;98%
With triethylamine In dichloromethane; water at 20℃; for 1.5h;52.7%
In ethanol
In water; ethyl acetate 1.) 0 deg C, 30 min, 2.) r.t., 2 h;
dimethyl amine
124-40-3

dimethyl amine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N,N-dimethyl-3-phenylpropanamide
5830-31-9

N,N-dimethyl-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere;100%
With triethylamine In diethyl ether93%
With triethylamine In diethyl ether Inert atmosphere;93%
Benzyloxymethyl-oxiran
2930-05-4

Benzyloxymethyl-oxiran

dimethyl amine
124-40-3

dimethyl amine

(+/-)-dimethyl<2-hydroxy-3-(benzyloxy)propyl>amine
97807-83-5

(+/-)-dimethyl<2-hydroxy-3-(benzyloxy)propyl>amine

Conditions
ConditionsYield
In tetrahydrofuran; water for 2h; Heating;100%
1,8-naphtholactone
5247-85-8

1,8-naphtholactone

dimethyl amine
124-40-3

dimethyl amine

N,N-Dimethyl-8-hydroxy-naphthalin-1-carboxamid
69674-57-3

N,N-Dimethyl-8-hydroxy-naphthalin-1-carboxamid

Conditions
ConditionsYield
In toluene Heating;100%
6-chloro-N,N'-diphenyl-1,3,5-triazine-2,4-diamine
1973-09-7

6-chloro-N,N'-diphenyl-1,3,5-triazine-2,4-diamine

dimethyl amine
124-40-3

dimethyl amine

N,N’-diphenyl-6-(isopropylamino)-[1,3,5]triazine-2,4-diamine
7710-42-1

N,N’-diphenyl-6-(isopropylamino)-[1,3,5]triazine-2,4-diamine

Conditions
ConditionsYield
With water; sodium carbonate for 1.5h; Heating;100%
ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle
52813-87-3

ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

dimethyl amine
124-40-3

dimethyl amine

ethylthio-8 trimethyl-N,N,5 5H-dibenzazepine-10-acetamide
52813-88-4

ethylthio-8 trimethyl-N,N,5 5H-dibenzazepine-10-acetamide

Conditions
ConditionsYield
In chloroform for 1h; Ambient temperature;100%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

dimethyl amine
124-40-3

dimethyl amine

N,N,2-trimethylbenzamide
6639-19-6

N,N,2-trimethylbenzamide

Conditions
ConditionsYield
100%
In water; toluene
In diethyl ether at 20℃; for 16h;
5-methyl-3-(methylsulfanyl)-1,2,4-triazine
28735-24-2

5-methyl-3-(methylsulfanyl)-1,2,4-triazine

dimethyl amine
124-40-3

dimethyl amine

N,N,5-trimethyl-1,2,4-triazin-3-amine
115125-15-0

N,N,5-trimethyl-1,2,4-triazin-3-amine

Conditions
ConditionsYield
In water a.) RT, 12 h b.) 70 deg C, 30 min;100%
formaldehyd
50-00-0

formaldehyd

6,7,8,9-tetrahydrobenzoindole
67720-26-7

6,7,8,9-tetrahydrobenzoindole

dimethyl amine
124-40-3

dimethyl amine

3-dimethylaminomethyl-6,7,8,9-tetrahydrobenzoindole
110595-87-4

3-dimethylaminomethyl-6,7,8,9-tetrahydrobenzoindole

Conditions
ConditionsYield
In acetic acid at 80℃; for 0.166667h;100%
formaldehyd
50-00-0

formaldehyd

dimethyl amine
124-40-3

dimethyl amine

1,3-Bis(3-thienyloxy)propane
155330-95-3

1,3-Bis(3-thienyloxy)propane

{3-[3-(2-Dimethylaminomethyl-thiophen-3-yloxy)-propoxy]-thiophen-2-ylmethyl}-dimethyl-amine

{3-[3-(2-Dimethylaminomethyl-thiophen-3-yloxy)-propoxy]-thiophen-2-ylmethyl}-dimethyl-amine

Conditions
ConditionsYield
With acetic acid Mannich reaction; Heating;100%
With acetic acid
formaldehyd
50-00-0

formaldehyd

dimethyl amine
124-40-3

dimethyl amine

C14H18O4S2
155330-77-1

C14H18O4S2

[3-(2-{2-[2-(2-Dimethylaminomethyl-thiophen-3-yloxy)-ethoxy]-ethoxy}-ethoxy)-thiophen-2-ylmethyl]-dimethyl-amine

[3-(2-{2-[2-(2-Dimethylaminomethyl-thiophen-3-yloxy)-ethoxy]-ethoxy}-ethoxy)-thiophen-2-ylmethyl]-dimethyl-amine

Conditions
ConditionsYield
With acetic acid at 20℃; for 48h; Mannich reaction;100%
With acetic acid
formaldehyd
50-00-0

formaldehyd

dimethyl amine
124-40-3

dimethyl amine

(+/-)-3-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-4,4-dimethyl-3,4-dihydro-2H,10H-<1,4>dioxepino<2,3-g>indole
172226-45-8

(+/-)-3-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-4,4-dimethyl-3,4-dihydro-2H,10H-<1,4>dioxepino<2,3-g>indole

(+/-)-3-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-4,4-dimethyl-8-<(N,N-dimethylamino)methyl>-3,4-dihydro-2H,10H-<1,4>dioxepino<2,3-g>indole
172226-24-3

(+/-)-3-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-4,4-dimethyl-8-<(N,N-dimethylamino)methyl>-3,4-dihydro-2H,10H-<1,4>dioxepino<2,3-g>indole

Conditions
ConditionsYield
In water; acetic acid for 24h;100%
With acetic acid99%
With acetic acid99%
(Z)-9-octadecenoyl chloride
112-77-6

(Z)-9-octadecenoyl chloride

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyl oleamide
2664-42-8

N,N-dimethyl oleamide

Conditions
ConditionsYield
In benzene for 1h; Ambient temperature;100%
In water for 1h; cooling;
Nonanoyl chloride
764-85-2

Nonanoyl chloride

dimethyl amine
124-40-3

dimethyl amine

octanecarboxylic acid dimethylamide
6225-08-7

octanecarboxylic acid dimethylamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 14h; Inert atmosphere;100%
In benzene 1.) 0 deg C, 1 h, 2.) r.t., 1h;90%

124-40-3Upstream product

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