2,6-Dicyclohexylnaphthalene

Base Information

• Chemical Name: 2,6-Dicyclohexylnaphthalene
• CAS No.: 42044-10-0
• Molecular Formula: C22H28
• Molecular Weight: 292.464
• DSSTox Substance ID: DTXSID70452299
• Nikkaji Number: J501.891I
• Wikidata: Q82272839
• Mol file: 42044-10-0.mol

Synonyms:2,6-dicyclohexylnaphthalene;Naphthalene, 2,6-dicyclohexyl-;42044-10-0;DTXSID70452299

Chemical Property of 2,6-Dicyclohexylnaphthalene

Chemical Property:

• XLogP3: 8.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 292.219100893
• Heavy Atom Count: 22
• Complexity: 300

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)C2=CC3=C(C=C2)C=C(C=C3)C4CCCCC4

Technology Process of 2,6-Dicyclohexylnaphthalene

There total 9 articles about 2,6-Dicyclohexylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

naphthalene (91-20-3,71998-51-1,72931-45-4) + cyclohexene (110-83-8) → 1-cyclohexylnaphthalene (3042-69-1) + 2-cyclohexylnaphthalene (42044-07-5) + 2,6-Dicyclohexylnaphthalene (42044-10-0) + 2,7-Dicyclohexylnaphthalene (136288-21-6)

Guidance literature:

zeolite HY_2.5; at 200 ℃; for 0.416667h; Yield given. Yields of byproduct given;

DOI:10.1021/jo00044a052

Reference yield:

1-bromocyclohexane (108-85-0) + naphthalene (91-20-3,71998-51-1,72931-45-4) → 1-cyclohexylnaphthalene (3042-69-1) + 2-cyclohexylnaphthalene (42044-07-5) + 2,6-Dicyclohexylnaphthalene (42044-10-0) + 2,7-Dicyclohexylnaphthalene (136288-21-6)

Guidance literature:

zeolite HY_2.5; at 82 ℃; for 6h; Product distribution; Mechanism; other catalysts, other temperature, other alkylating agent;

DOI:10.1021/jo00044a052

Reference yield:

naphthalene (91-20-3,71998-51-1,72931-45-4) + cyclohexanol (108-93-0) → 2,6-Dicyclohexylnaphthalene (42044-10-0)

Guidance literature:

With boron trifluoride;

DOI:10.1002/1521-4052(200006)31:6<440::AID-MAWE440>3.0.CO;2-7 DOI:10.1021/ja01277a062

upstream raw materials:

naphthalene

cyclohexene

cyclohexanol

1-bromocyclohexane

Downstream raw materials:

[Zn(mthd)₂(bpy)]