1,12-DIACETOXYDODECANE

Base Information

• Chemical Name: 1,12-DIACETOXYDODECANE
• CAS No.: 42236-50-0
• Molecular Formula: C16H30O4
• Molecular Weight: 286.412
• Hs Code.: 2915390090
• Mol file: 42236-50-0.mol

Synonyms:12-acetyloxydodecyl acetate;1,12-Dodecanediol Diacetate;Dodecamethylene Diacetate;

Chemical Property of 1,12-DIACETOXYDODECANE

Chemical Property:

• Vapor Pressure: 0.000213mmHg at 25°C
• Melting Point: 40oC
• Boiling Point: 190oC / 10mmHg
• Flash Point: 146.4oC
• PSA: 52.60000
• Density: 0.955g/cm3
• LogP: 4.01360
• Storage Temp.: 0-10°C
• Solubility.: soluble in Toluene

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,12-Diacetoxydodecane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,12-DIACETOXYDODECANE

There total 7 articles about 1,12-DIACETOXYDODECANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

dodec-11-en-1-ol (35289-31-7) + acetic anhydride (108-24-7) → 1,12-diacetoxydodecane (42236-50-0)

Guidance literature:

With sulfuric acid; at 50 ℃; for 1h;

DOI:10.1007/BF00580036

Reference yield:

1,12-dibromododecane (3344-70-5) + potassium acetate (127-08-2) → 1,12-diacetoxydodecane (42236-50-0)

Guidance literature:

With acetic acid;

Reference yield:

1,12-dodecandiol (5675-51-4) → 1,12-diacetoxydodecane (42236-50-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / stearic acid, palmitic acid / 350 °C / 260 Torr

2: 93 percent / H₂SO₄ / 1 h / 50 °C

With sulfuric acid; 1-hexadecylcarboxylic acid; stearic acid;

DOI:10.1007/BF00580036

upstream raw materials:

1,12-dibromododecane

potassium acetate

silver(I) acetate

dodec-11-en-1-ol

Downstream raw materials:

dodec-11-en-1-ol

cis-11-tetradecen-1-ol

(Z)-11-hexadecen-1-ol

13-tetradec-11-yn-1-ol