Benzenamine, N,N-dimethyl-4-(2-methyl-1-propenyl)-

Base Information

Chemical Name:Benzenamine, N,N-dimethyl-4-(2-methyl-1-propenyl)-
CAS No.:4278-80-2
Molecular Formula:C12H17N
Molecular Weight:175.274
Hs Code.:2921430090
Mol file:4278-80-2.mol

Synonyms:N,N-dimethyl-p-2',2'-dimethylvinylaniline;N,N-dimethyl-4-(2-methyl-propenyl)-aniline;N,N-Dimethyl-4-(2-methyl-propenyl)-anilin;β-Methyl-α-(4-dimethylamino-phenyl)-α-propylen;N.N-Dimethyl-4-(β.β-dimethyl-vinyl)-anilin;

Suppliers and Price of Benzenamine, N,N-dimethyl-4-(2-methyl-1-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Benzenamine, N,N-dimethyl-4-(2-methyl-1-propenyl)-

Chemical Property:

PSA：3.24000
LogP:3.17580

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenamine, N,N-dimethyl-4-(2-methyl-1-propenyl)-

There total 2 articles about Benzenamine, N,N-dimethyl-4-(2-methyl-1-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 513-37-1
2-methylprop-1-enyl chloride

: 7353-91-5
4-dimethylaminophenylmagnesium bromide

: 4278-80-2
N,N-dimethyl-4-(2-methylprop-1-en-1-yl)aniline

Guidance literature:: With C₃₂H₂₆ClN₂NiP; In tetrahydrofuran; at 30 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1055/s-0033-1339653

Reference yield:

: 100-10-7
4-dimethylamino-benzaldehyde

: 4278-80-2
N,N-dimethyl-4-(2-methylprop-1-en-1-yl)aniline

Guidance literature:: With hexamethyldisilazide; Yield given. Multistep reaction; 1.) THF, r.t., 30 min, 2.) THF, r.t., 20 min;
DOI:10.1039/a803612h

Reference yield: 86.0%

: 127571-48-6,159248-17-6
cis-[Os(VI)(2,2':6',2''-terpyridine)(Cl)2(N)](PF₆)

: 4278-80-2
N,N-dimethyl-4-(2-methylprop-1-en-1-yl)aniline

: cis-[(2,2':6',2''-terpyridine)OsCl2(η2-(C,N)-[Me2NC6H4]CH=N=CMe2)]PF6

Guidance literature:: In acetonitrile; soln. of Os-complex and ligand in MeCN was added into flask, allowed to stand at room temp. for 1 h under N2 or Ar; MeCN was evapd. on rotary evaporator, layered with ether, allowed to stand overnight at -20°C, filtered, washed with Et2O, dried in air; elem. anal.;
DOI:10.1021/om034404m