2-(3-CHLOROPHENYL)-2-OXOETHYL THIOCYANATE

Base Information

• Chemical Name: 2-(3-CHLOROPHENYL)-2-OXOETHYL THIOCYANATE
• CAS No.: 43045-12-1
• Molecular Formula: C9H6ClNOS
• Molecular Weight: 0.00000
• Hs Code.: 2930909899
• Mol file: 43045-12-1.mol

Synonyms:

Chemical Property of 2-(3-CHLOROPHENYL)-2-OXOETHYL THIOCYANATE

Chemical Property:

• Melting Point: 87-89
• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

98%min ^*data from raw suppliers

2-(3-Chlorophenyl)-2-oxoethylThiocyanate ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of 2-(3-CHLOROPHENYL)-2-OXOETHYL THIOCYANATE

There total 10 articles about 2-(3-CHLOROPHENYL)-2-OXOETHYL THIOCYANATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

ammonium thiocyanate + 3'-Chloroacetophenone (99-02-5) → 1-(3-chlorophenyl)-2-thiocyanatoethan-1-one (43045-12-1)

Guidance literature:

With Selectfluor; In acetonitrile; at 20 ℃; for 0.833333h; regioselective reaction;

DOI:10.1007/s12039-012-0270-0

Reference yield: 82.0%

ammonium thiocyanate (1147550-11-5) + 3'-Chloroacetophenone (99-02-5) → 1-(3-chlorophenyl)-2-thiocyanatoethan-1-one (43045-12-1)

Guidance literature:

With Oxone; In methanol; at 20 ℃; for 6h;

DOI:10.1080/00397910802029349

Reference yield: 76.0%

3-Chlorostyrene (2039-85-2,26100-04-9) + ammonium thiocyanate (1147550-11-5) → 1-(3-chlorophenyl)-2-thiocyanatoethan-1-one (43045-12-1)

Guidance literature:

With oxygen; In ethanol; at 20 ℃;

upstream raw materials:

ammonium thiocyanate

3'-Chloroacetophenone

2-bromo-1-(3-chloro-phenyl)-ethanone

potassium thioacyanate

Downstream raw materials:

C₉H₆ClNOS

[3-(p-tolyl)thiophene-2,5-diyl]bis[(3-chlorophenyl)methanone]

[3-(4-methoxyphenyl)thiophene-2,5-diyl]bis[(3-chlorophenyl)methanone]

[3-(3,4-dimethoxyphenyl)thiophene-2,5-diyl]bis[(3-chlorophenyl)methanone]

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