Trichothec-9-en-8-one, 3,15-bis(acetyloxy)-12,13-epoxy-7-hydroxy-, (3alpha,7alpha)-

Base Information

Chemical Name:Trichothec-9-en-8-one, 3,15-bis(acetyloxy)-12,13-epoxy-7-hydroxy-, (3alpha,7alpha)-
CAS No.:56676-60-9
Molecular Formula:C19H24O8
Molecular Weight:380.3891
Hs Code.:
UNII:S7W3YU5F6G
Nikkaji Number:J579.948A
Wikidata:Q27288794

Synonyms:3,15-diacetyldeoxynivalenol;3,15-diacetyldeoxynivalenol, (3alpha,7alpha)-isomer

Suppliers and Price of Trichothec-9-en-8-one, 3,15-bis(acetyloxy)-12,13-epoxy-7-hydroxy-, (3alpha,7alpha)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of Trichothec-9-en-8-one, 3,15-bis(acetyloxy)-12,13-epoxy-7-hydroxy-, (3alpha,7alpha)-

Chemical Property:

Vapor Pressure:3.86E-13mmHg at 25°C
Boiling Point:523.3°C at 760 mmHg
Flash Point:184.3°C
PSA：111.66000
Density:1.38g/cm³
LogP:0.30390
XLogP3:-0.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:5
Exact Mass:380.14711772
Heavy Atom Count:27
Complexity:759

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2C(C(C1=O)O)(C3(CC(C(C34CO4)O2)OC(=O)C)C)COC(=O)C
Isomeric SMILES:CC1=C[C@@H]2[C@]([C@@H](C1=O)O)([C@]3(C[C@H]([C@H]([C@@]34CO4)O2)OC(=O)C)C)COC(=O)C

Technology Process of Trichothec-9-en-8-one, 3,15-bis(acetyloxy)-12,13-epoxy-7-hydroxy-, (3alpha,7alpha)-

There total 8 articles about Trichothec-9-en-8-one, 3,15-bis(acetyloxy)-12,13-epoxy-7-hydroxy-, (3alpha,7alpha)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 108-24-7
acetic anhydride

: 51481-10-8,50722-37-7,115825-61-1
vomitoxin

: 88337-96-6
15-acetoxy-3,7-dihydroxy-12,13-epoxytrichothec-9-en-8-one

: 56676-60-9,99604-10-1
3,15-diacetyldeoxynivalenol

Guidance literature:: With pyridine; dmap; In dichloromethane; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2014.05.064

Reference yield:

: 108-24-7
acetic anhydride

: 51481-10-8,50722-37-7,115825-61-1
vomitoxin hydrate

: 88337-96-6
C₁₇H₂₂O₇

: 56676-60-9
C₁₉H₂₄O₈

: 50722-38-8,115825-62-2
3α-acetoxy-7α,15-dihydroxy-12,13-epoxytrichothec-9-en-8-one

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 5h; Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo00251a040