ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate

Base Information

Chemical Name:ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate
CAS No.:443956-09-0
Molecular Formula:C9H9BrN2O5
Molecular Weight:305.085
Hs Code.:
Mol file:443956-09-0.mol

Synonyms:ethyl (6-bromo-2-nitro-pyridin-3-yl-oxy)acetate;ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate;ethyl [(6-bromo-2-nitropyridin-3-yl)oxy]acetate;(6-bromo-2-nitropyridin-3-yloxy)acetic acid ethyl ester;(6-bromo-2-nitro-pyridin-3-yloxy)-acetic acid ethyl ester;ethyl (6-bromo-2-nitropyridin-3-yloxy)acetate;

Suppliers and Price of ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

A1 Biochem Labs
Aceticacid,[(6-bromo-2-nitro-3-pyridinyl)oxy]-,ethylester 95%
1 g
$ 600.00

Total 2 raw suppliers

Chemical Property of ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate

Chemical Property:

PSA：94.24000
LogP:2.21740

Purity/Quality:

99%min ^*data from raw suppliers

Aceticacid,[(6-bromo-2-nitro-3-pyridinyl)oxy]-,ethylester 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate

There total 2 articles about ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 443956-08-9
6-bromo-2-nitropyridin-3-ol

: 105-36-2
ethyl bromoacetate

: 443956-09-0
ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate

Guidance literature:: With potassium carbonate; In acetone; for 10h; Heating / reflux;

Reference yield:

: 15128-82-2
3-hydroxy-2-nitropyridine

: 443956-09-0
ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 5 h / 25 °C

With N-Bromosuccinimide; potassium carbonate; In N,N-dimethyl-formamide;

Reference yield: 67.7%

: 443956-09-0
ethyl 2-(6-bromo-2-nitropyridin-3-yloxy)acetate

: benzyl N-[rac-3a,7a-trans-6,7a-cis-2-oxo-3a,4,5,6,7,7a-hexahydro-3H-1,3-benzoxazol-6-yl]carbamate

: ethyl 2-[2-nitro-6-[rac-3a,7a-trans-6,7a-cis-2-oxo-6-(phenylmethoxycarbonylamino)-3a,4,5,6,7,7a-hexahydro-1,3-benzoxazol-3-yl]pyridin-3-yl]oxyacetate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; at 100 ℃; for 2h;