tert-butyl allyl[(4-methylphenyl)sulfonyl]carbamate

Base Information

Chemical Name:tert-butyl allyl[(4-methylphenyl)sulfonyl]carbamate
CAS No.:462996-06-1
Molecular Formula:C15H21NO4S
Molecular Weight:311.402
Hs Code.:
Mol file:462996-06-1.mol

Synonyms:tert-butyl allyl(tosyl)carbamate;N-allyl-N-(t-butoxycarbonyl)-p-toluenesulfonamide;

Suppliers and Price of tert-butyl allyl[(4-methylphenyl)sulfonyl]carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl allyl[(4-methylphenyl)sulfonyl]carbamate

Chemical Property:

PSA：72.06000
LogP:4.18760

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-butyl allyl[(4-methylphenyl)sulfonyl]carbamate

There total 3 articles about tert-butyl allyl[(4-methylphenyl)sulfonyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 106-95-6
allyl bromide

: 462996-06-1
N-allyl-N-tert-butoxycarbonyl-p-toluenesulfonamide

Guidance literature:: With potassium carbonate; In acetonitrile; for 1.5h; Heating;
DOI:10.1002/anie.200454157

Reference yield: 98.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 50487-71-3
4-methyl-N-(2-propenyl)benzenesulfonamide

: 462996-06-1
N-allyl-N-tert-butoxycarbonyl-p-toluenesulfonamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/ol901901m

Reference yield:

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 107-18-6
allyl alcohol

: 462996-06-1
N-allyl-N-tert-butoxycarbonyl-p-toluenesulfonamide

Guidance literature:: With PhP(C₆H₄-p-(CH₂)2C₆F₁₃)2; bis(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)diazo dicarboxylate; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1016/S0040-4020(02)00205-3