3-(1-Methylethoxy)-2-butenoic acid ethyl ester

Base Information

Chemical Name:3-(1-Methylethoxy)-2-butenoic acid ethyl ester
CAS No.:1540-21-2
Molecular Formula:C9H16 O3
Molecular Weight:172.224
Hs Code.:2918990090
European Community (EC) Number:216-267-3
Nikkaji Number:J206.763C
Mol file:1540-21-2.mol

Synonyms:3-(1-Methylethoxy)-2-butenoic acid ethyl ester;ethyl (Z)-3-propan-2-yloxybut-2-enoate;1540-21-2

Suppliers and Price of 3-(1-Methylethoxy)-2-butenoic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-(1-Methylethoxy)-2-butenoic acid ethyl ester

Chemical Property:

Vapor Pressure:0.0966mmHg at 25°C
Boiling Point:223.4°C at 760 mmHg
Flash Point:85.7°C
PSA：35.53000
Density:0.952g/cm³
LogP:1.87830
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:172.109944368
Heavy Atom Count:12
Complexity:171

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C=C(C)OC(C)C
Isomeric SMILES:CCOC(=O)/C=C(/C)\OC(C)C

Technology Process of 3-(1-Methylethoxy)-2-butenoic acid ethyl ester

There total 6 articles about 3-(1-Methylethoxy)-2-butenoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 141-97-9
ethyl acetoacetate

: 67-63-0,8013-70-5
isopropyl alcohol

: 1540-21-2
ethyl 3-isopropoxy-2-butenoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at -20 ℃; for 48h;
DOI:10.1246/bcsj.54.2107

Reference yield:

: 141-97-9
ethyl acetoacetate

: 67-63-0,8013-70-5
isopropyl alcohol

: 1972-28-7,218603-74-8
diethylazodicarboxylate

: 1540-21-2
ethyl 3-isopropoxy-2-butenoate

: 3-<1,2-bis(ethoxycarbonyl)hydrazino>-2-butenoate

: 3-<2-isopropyl-1,2-bis(ethoxycarbonyl)hydrazino>-2-butenoate

Guidance literature:: With triphenylphosphine; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, 2.) THF, -20 deg C, 2 d;
DOI:10.1246/bcsj.54.2107