N-Methoxy-2,N-diMethyl-nicotinaMide

Base Information

Chemical Name:N-Methoxy-2,N-diMethyl-nicotinaMide
CAS No.:469864-28-6
Molecular Formula:C9H12N2O2
Molecular Weight:180.206
Hs Code.:
Mol file:469864-28-6.mol

Synonyms:N-METHOXY-N,2-DIMETHYLNICOTINAMIDE;2-methylnicotinic acid methoxymethylamide;N-methoxy-2,N-dimethyl-nicotinamide;

Suppliers and Price of N-Methoxy-2,N-diMethyl-nicotinaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
N-Methoxy-N,2-dimethylpyridine-3-carboxamide 95%
5g
$ 1320.00

Crysdot
N-Methoxy-N,2-dimethylnicotinamide 97%
5g
$ 980.00

Crysdot
N-Methoxy-N,2-dimethylnicotinamide 97%
10g
$ 1400.00

Crysdot
N-Methoxy-N,2-dimethylnicotinamide 97%
1g
$ 380.00

Alichem
N-Methoxy-N,2-dimethylnicotinamide
10g
$ 1442.00

Alichem
N-Methoxy-N,2-dimethylnicotinamide
5g
$ 1029.00

A1 Biochem Labs
N-methoxy-N,2-dimethylpyridine-3-carboxamide 95%
5 g
$ 800.00

Total 2 raw suppliers

Chemical Property of N-Methoxy-2,N-diMethyl-nicotinaMide

Chemical Property:

Boiling Point:331.0±30.0 °C(Predicted)
PKA:3.88±0.10(Predicted)
PSA：42.43000
Density:1.122±0.06 g/cm3(Predicted)
LogP:1.02340

Purity/Quality:

99% ^*data from raw suppliers

N-Methoxy-N,2-dimethylpyridine-3-carboxamide 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Methoxy-2,N-diMethyl-nicotinaMide

There total 2 articles about N-Methoxy-2,N-diMethyl-nicotinaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3222-56-8
2-methylnicotinic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 469864-28-6
2-methylnicotinic acid methoxymethylamide

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 - 23 ℃;
DOI:10.1021/jacs.9b10414

Reference yield:

: 3222-56-8
2-methylnicotinic acid

: 469864-28-6
2-methylnicotinic acid methoxymethylamide

Guidance literature:: With N,O-dimethylhydroxylamine*hydrochloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; acetonitrile;

Reference yield: 72.0%

: 469864-28-6
2-methylnicotinic acid methoxymethylamide

: 38749-79-0
3-bromo-2-picoline

: bis(2-methylpyridin-3-yl)methanone

Guidance literature:: 3-bromo-2-picoline; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

2-methylnicotinic acid methoxymethylamide; In tetrahydrofuran; diethyl ether; hexane; at -78 - -20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1021/jacs.9b10414