6-Methoxy-alpha-(4-nitrophenylimino)-O-cresol

Base Information

• Chemical Name: 6-Methoxy-alpha-(4-nitrophenylimino)-O-cresol
• CAS No.: 47074-10-2
• Molecular Formula: C14H12N2O4
• Molecular Weight: 272.25600
• European Community (EC) Number: 666-129-5
• DSSTox Substance ID: DTXSID00425451
• Mol file: 47074-10-2.mol

Synonyms:2-methoxy-6-{(E)-[(4-nitrophenyl)imino]methyl}phenol;47074-10-2;ZINC04672246;6-METHOXY-ALPHA-(4-NITROPHENYLIMINO)-O-CRESOL;DTXSID00425451;STK083339;AKOS005392959

Chemical Property of 6-Methoxy-alpha-(4-nitrophenylimino)-O-cresol

Chemical Property:

• PSA: 84.15000
• LogP: 3.15600
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 272.07970687
• Heavy Atom Count: 20
• Complexity: 348

Purity/Quality:

6-METHOXY-ALPHA-(4-NITROPHENYLIMINO)-ORTHO-CRESOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=CC(=C1O)C=NC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 6-Methoxy-alpha-(4-nitrophenylimino)-O-cresol

There total 1 articles about 6-Methoxy-alpha-(4-nitrophenylimino)-O-cresol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxy-2-hydroxybenzaldehyde (148-53-8) + 4-nitro-aniline (100-01-6,104810-17-5) → 3-Methoxy-2-hydroxybenzyliden-p-nitranilin (47074-10-2)

Guidance literature:

In ethanol; for 5h; Heating;

DOI:10.1016/S0022-2860(03)00453-8

Reference yield: 78.0%

copper(II) choride dihydrate + ethanol (64-17-5) + 3-Methoxy-2-hydroxybenzyliden-p-nitranilin (47074-10-2) → C28H22CuN4O8*2C2H6O

Guidance literature:

for 0.5h; Heating;

DOI:10.4314/BCSE.V35I1.3

Reference yield: 33.0%

3-Methoxy-2-hydroxybenzyliden-p-nitranilin (47074-10-2) → C28H22N4O8(1+)*ClO4(1-)

Guidance literature:

With sodium perchlorate; In acetonitrile; Ambient temperature; glassy carbon plate anode, platinum foil cathode; 1.00 V;

upstream raw materials:

3-methoxy-2-hydroxybenzaldehyde

4-nitro-aniline