1-tetradecyl-3-methylimidazolium bromide

Base Information

• Chemical Name: 1-tetradecyl-3-methylimidazolium bromide
• CAS No.: 471907-87-6
• Molecular Formula: Br*C₁₈H₃₅N₂
• Molecular Weight: 359.393
• Mol file: 471907-87-6.mol

Synonyms:1-methyl-3-tetradecyl-1,2-dihydroimidazol-1-ium,bromide;1-tetradecyl-3-methylimidazolium bromide;

Chemical Property of 1-tetradecyl-3-methylimidazolium bromide

Chemical Property:

• Melting Point: 56℃
• PSA: 6.48000
• LogP: 6.19750

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-tetradecyl-3-methylimidazolium bromide

There total 1 articles about 1-tetradecyl-3-methylimidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-methyl-1H-imidazole (616-47-7) + 1-Bromotetradecane (112-71-0) → 1‐tetradecyl‐3‐methylimidazolium bromide (471907-87-6)

Guidance literature:

In toluene; at 80 ℃; for 24h;

DOI:10.1016/j.molliq.2020.113206

Reference yield:

1‐tetradecyl‐3‐methylimidazolium bromide (471907-87-6) → 1-tetradecyl-3-methylimidazolium ortho-methoxycinnate

Guidance literature:

Multi-step reaction with 3 steps

1: Ambersep 900(OH) anion exchange resin / water

2: water

3: water / 24.84 °C / UV-irradiation

With Ambersep 900(OH) anion exchange resin; In water;

DOI:10.1039/c4cc04274c

upstream raw materials:

1-methyl-1H-imidazole

1-Bromotetradecane

Refernces

• 1、 Pal, Amalendu,Yadav, Sangeeta. "Effect of anionic polyelectrolyte sodium carboxymethylcellulose on the aggregation behavior of surface active ionic liquids in aqueous solution". . p. 584 - 594. Retrieved 2017.
• 2、 Nozaki, Yoko,Yamaguchi, Keito,Tomida, Kenji,Taniguchi, Natsumi,Hara, Hironori,Takikawa, Yoshinori,Sadakane, Koichiro,Nakamura, Kenji,Konishi, Takashi,Fukao, Koji. "Phase Transition and Dynamics in Imidazolium-Based Ionic Liquid Crystals through a Metastable Highly Ordered Smectic Phase". . p. 5291 - 5300. Retrieved 2016.
• 3、 Luo, Genxiang,Qi, Xinjie,Han, Chunyu,Liu, Chunsheng,Gui, Jianzhou. "Salt effect on mixed micelle and interfacial properties of conventional cationic surfactants and the ionic liquid surfactant 1-tetradecyl-3- methylimidazolium bromide ([C14mim]Br)". . p. 531 - 538. Retrieved 2013.
• 4、 Kumar, Harsh,Sharma, Pooja. "Investigations on the micellization behavior and thermodynamic characteristics of synthesized surface active ionic liquids [C14mim] [Br] and [C15mim] [Br] in the presence of oral antidiabetic drug metformin hydrochloride". . . Retrieved 2021.
• 5、 Kaur, Ramanjeet,Kumar, Harsh. "Exploration of the soluting-out effect of carbohydrates on the micellization and surface activity of long-chain imidazolium ionic liquid in the aqueous medium". . . Retrieved 2020.