Stannane, [1,4-phenylenebis(methylene)]bis[trichloro-

Base Information

Chemical Name:Stannane, [1,4-phenylenebis(methylene)]bis[trichloro-
CAS No.:476014-59-2
Molecular Formula:C₈H₈Cl₆Sn₂
Molecular Weight:554.29
Hs Code.:

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Chemical Property of Stannane, [1,4-phenylenebis(methylene)]bis[trichloro-

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Technology Process of Stannane, [1,4-phenylenebis(methylene)]bis[trichloro-

There total 1 articles about Stannane, [1,4-phenylenebis(methylene)]bis[trichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 476014-54-7
1,4-bis(tricyclohexylstannylmethyl)benzene

: 7646-78-8
tin(IV) chloride

: 476014-59-2
1,4-bis(trichlorostannylmethyl)benzene

Guidance literature:: In toluene; SnCl4 was added to a soln. of bis(tricyclohexylstannylated) comound at -30°C (N2); the solvent was evapd., recrystd. from THF/CH2Cl2; elem. anal.;
DOI:10.1021/om0202468

Reference yield: 73.0%

: 476014-59-2
1,4-bis(trichlorostannylmethyl)benzene

: 1666-13-3
diphenyl diselenide

: 1,4-bis[tris(selenophenolato)stannylmethyl]benzene

Guidance literature:: With NaBH₄; In ethanol; byproducts: NaCl; under Ar or N2; Ph2Se2 dissolved in degassed abs. EtOH; NaBH4 (6 equiv.)added in small portions; Sn compd. in EtOH added slowly at 0°C; stirred for 24 h; filtered; washed with EtOH and hexane; dried in vac.; crystd. from CH2Cl2-hexane over 1 wk;
DOI:10.1002/zaac.200800263