Benzenamine, N,N'-(1,10-phenanthroline-2,9-diyldimethylidyne)bis[2,6-bis(1-methyleth yl)-

Base Information

Chemical Name:Benzenamine, N,N'-(1,10-phenanthroline-2,9-diyldimethylidyne)bis[2,6-bis(1-methyleth yl)-
CAS No.:478813-34-2
Molecular Formula:C₃₈H₄₂N₄
Molecular Weight:554.778
Hs Code.:

Synonyms:

Suppliers and Price of Benzenamine, N,N'-(1,10-phenanthroline-2,9-diyldimethylidyne)bis[2,6-bis(1-methyleth yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzenamine, N,N'-(1,10-phenanthroline-2,9-diyldimethylidyne)bis[2,6-bis(1-methyleth yl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenamine, N,N'-(1,10-phenanthroline-2,9-diyldimethylidyne)bis[2,6-bis(1-methyleth yl)-

There total 1 articles about Benzenamine, N,N'-(1,10-phenanthroline-2,9-diyldimethylidyne)bis[2,6-bis(1-methyleth yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 24544-04-5
2,6-diisopropylbenzenamine

: 57709-62-3
1,10-phenanthroline-2,9-dicarboxaldehyde

: 478813-34-2
2,9-bis[(2,6-diisopropylphenylimino)methyl]phenanthroline

Guidance literature:: With acetic acid; In ethanol; for 5h; Heating;
DOI:10.1016/S0022-328X(02)01623-6

Reference yield: 86.0%

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 75-09-2
dichloromethane

: 478813-34-2
2,9-bis[(2,6-diisopropylphenylimino)methyl]phenanthroline

: dibromo[2,9-diformyl-1,10-phenanthrolinebis(2,6-diisopropylanil)]nickel(II)*(dichloromethane)

Guidance literature:: In dichloromethane; under N2; CH2Cl2 added to mixt. of Ni complex and ligand (molar ratio 1:1.2); stirred at room temp. for 18 h; concd. to half of vol.; Et2O added; ppt. washed with Et2O; filtered; dried; elem. anal.;
DOI:10.1016/S0022-328X(02)01623-6

Reference yield: 73.0%

: iron(II) chloride

: 478813-34-2
2,9-bis[(2,6-diisopropylphenylimino)methyl]phenanthroline

: 478813-02-4
1,9-bis[(2,6-diisopropylphenylimino)methyl]phenanthrolineiron dichloride

Guidance literature:: In tetrahydrofuran; under N2; ligand (1 equiv.) added to soln. of FeCl2 in THF; stirred at room temp. overnight; solvent removed in vac.; washed with Et2O; elem. anal.;
DOI:10.1016/S0020-1693(02)01293-8