3-Methoxy-6-methylpyridin-2-amine

Base Information

• Chemical Name: 3-Methoxy-6-methylpyridin-2-amine
• CAS No.: 478913-57-4
• Molecular Formula: C7H10N2O
• Molecular Weight: 138.16700
• Hs Code.: 2933399090
• European Community (EC) Number: 830-896-6
• DSSTox Substance ID: DTXSID10587498
• Wikidata: Q82479945
• Mol file: 478913-57-4.mol

Synonyms:3-METHOXY-6-METHYLPYRIDIN-2-AMINE;478913-57-4;2-amino-3-methoxy-6-methylpyridine;2-Pyridinamine,3-methoxy-6-methyl-(9CI);MFCD09878490;3-methoxy-6-methyl-2-pyridinylamine;SCHEMBL259054;DTXSID10587498;GCVWQZUQWGOTKH-UHFFFAOYSA-N;3-Methoxy-6-methylpyridin-2-ylamine;AKOS011378882;CCG-302516;MCULE-8380689549;SB75587;AS-42295;SY193843;DB-121976;CS-0145993;EN300-97912;AP-501/43408348;Z955136104

Chemical Property of 3-Methoxy-6-methylpyridin-2-amine

Chemical Property:

• PSA: 48.14000
• LogP: 1.56200
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature
• XLogP3: 0.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 138.079312947
• Heavy Atom Count: 10
• Complexity: 108

Purity/Quality:

99%, ^*data from raw suppliers

3-methoxy-6-methylpyridin-2-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=NC(=C(C=C1)OC)N

Technology Process of 3-Methoxy-6-methylpyridin-2-amine

There total 3 articles about 3-Methoxy-6-methylpyridin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxy-6-methyl-2-nitro-pyridine (24015-98-3) → 2-amino-3-methoxy-6-methylpyridine (478913-57-4)

Guidance literature:

With hydrogen; palladium on activated carbon; In ethanol; for 2h;

Reference yield:

methyl iodide (74-88-4) + 6-methyl-2-nitropyridin-3-ol (15128-90-2) → 2-amino-3-methoxy-6-methylpyridine (478913-57-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

6-methyl-2-nitropyridin-3-ol (15128-90-2) → 2-amino-3-methoxy-6-methylpyridine (478913-57-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2012.01.033

upstream raw materials:

3-methoxy-6-methyl-2-nitro-pyridine

methyl iodide

6-methyl-2-nitropyridin-3-ol

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