Butanal, 2-[(triphenylmethyl)amino]-, (2R)-

Base Information

Chemical Name:Butanal, 2-[(triphenylmethyl)amino]-, (2R)-
CAS No.:482615-37-2
Molecular Formula:C23H23NO
Molecular Weight:329.442
Hs Code.:

Synonyms:

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Chemical Property of Butanal, 2-[(triphenylmethyl)amino]-, (2R)-

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Technology Process of Butanal, 2-[(triphenylmethyl)amino]-, (2R)-

There total 2 articles about Butanal, 2-[(triphenylmethyl)amino]-, (2R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 176315-09-6
(R)-2-(trityl-amino)-butan-1-ol

: 482615-37-2
(R)-2-(trityl-amino)-butyraldehyde

Guidance literature:: (R)-2-(trityl-amino)-butan-1-ol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -45 ℃; for 4h;

With triethylamine; In dichloromethane; at -45 - 20 ℃; for 16h;

Reference yield:

: 76-83-5
trityl chloride

: 482615-37-2
(R)-2-(trityl-amino)-butyraldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 48 h / 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 3 h / -45 °C / Inert atmosphere

2.2: 16 h / -40 - 20 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; 2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1016/j.bmc.2011.08.051

Reference yield: 47.0%

: 482615-37-2
(R)-2-(trityl-amino)-butyraldehyde

: 1888-75-1
isopropyllithium

: (3RS,4R)-2-methyl-4-(tritylamino)hexan-3-ol

Guidance literature:: isopropyllithium; copper(I) bromide dimethylsulfide complex; In diethyl ether; pentane; at -78 - 20 ℃;

(R)-2-(trityl-amino)-butyraldehyde; In diethyl ether; pentane; at -70 - -55 ℃; for 4h;

With ammonium chloride; In diethyl ether; water; pentane; at -55 - 20 ℃; for 16h;