Mammea A/AD cyclo D

Base Information

Chemical Name:Mammea A/AD cyclo D
CAS No.:30563-62-3
Molecular Formula:C₂₅H₂₆O₆
Molecular Weight:422.478
Hs Code.:
Mol file:30563-62-3.mol

Synonyms:2H-Furo[2,3-h]-1-benzopyran-2-one,8,9-dihydro-5-hydroxy-8-(1-hydroxy-1-methylethyl)-6-isovaleryl-4-phenyl- (8CI);Cyclomammeisin; Mammea A/AA cyclo F

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Chemical Property of Mammea A/AD cyclo D

Chemical Property:

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Technology Process of Mammea A/AD cyclo D

There total 8 articles about Mammea A/AD cyclo D which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 18483-64-2
mammeisin

: 30563-62-3,111821-09-1,188817-92-7
4-phenyl-5-hydroxy-6-(3-methyl-1-oxobutyl)-2'-(1-hydroxy-1-methylethyl)-3',4'-dihydro(5',4':7,8)furanocoumarin

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; Ambient temperature;

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 30563-62-3,111821-09-1,188817-92-7
4-phenyl-5-hydroxy-6-(3-methyl-1-oxobutyl)-2'-(1-hydroxy-1-methylethyl)-3',4'-dihydro(5',4':7,8)furanocoumarin

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / AlCl₃ / CS₂; nitrobenzene / 0.5 h / Heating

2: cc. H₂SO₄ / acetic acid / 480 h / Ambient temperature

3: 20 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C

4: 58 percent / MCPBA / CH₂Cl₂ / Ambient temperature

With potassium hydroxide; aluminium trichloride; sulfuric acid; 3-chloro-benzenecarboperoxoic acid; In carbon disulfide; dichloromethane; acetic acid; nitrobenzene;

Reference yield:

: 98192-57-5
5,7-dihydroxy-6-(3-methylbutanoyl)-4-phenyl-2H-chromen-2-one

: 30563-62-3,111821-09-1,188817-92-7
4-phenyl-5-hydroxy-6-(3-methyl-1-oxobutyl)-2'-(1-hydroxy-1-methylethyl)-3',4'-dihydro(5',4':7,8)furanocoumarin

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C

2: 58 percent / MCPBA / CH₂Cl₂ / Ambient temperature

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;