3-[2-[[3-(2-carboxyethyl)-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-2-yl]methyl]-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-3-yl]propanoic acid

Base Information

Chemical Name:3-[2-[[3-(2-carboxyethyl)-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-2-yl]methyl]-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-3-yl]propanoic acid
CAS No.:79719-28-1
Molecular Formula:C₃₃H₄₀N₄O₆
Molecular Weight:588.704
Hs Code.:

3-[2-[[3-(2-carboxyethyl)-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-2-yl]methyl]-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-3-yl]propanoic acid

Synonyms:

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Chemical Property of 3-[2-[[3-(2-carboxyethyl)-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-2-yl]methyl]-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-3-yl]propanoic acid

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:900.945°C at 760 mmHg
Flash Point:498.674°C
Density:1.283g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-[2-[[3-(2-carboxyethyl)-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-2-yl]methyl]-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-3-yl]propanoic acid

There total 13 articles about 3-[2-[[3-(2-carboxyethyl)-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-2-yl]methyl]-5-[(Z)-(3-ethyl-4-methyl-5-oxo-pyrrol-2-ylidene)methyl]-4-methyl-1H-pyrrol-3-yl]propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 89332-47-8
mesobilirubin-XIIIα dimethyl ester

: 79719-28-1
3-{2-{3-(2-Carboxy-ethyl)-5-[3-ethyl-4-methyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-5-[3-ethyl-4-methyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; for 4h; Heating;
DOI:10.1055/s-1992-26102

Reference yield:

: 29790-14-5
mesobiliverdin XIII_α dimethylester

: 79719-28-1
3-{2-{3-(2-Carboxy-ethyl)-5-[3-ethyl-4-methyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-5-[3-ethyl-4-methyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaBH₄ / tetrahydrofuran; methanol / 20 °C / ultrasound

2: 97 percent / 1 M aq. NaOH / tetrahydrofuran; methanol / 4 h / Heating

With sodium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; methanol;
DOI:10.1055/s-1992-26102

Reference yield:

: 64845-01-8
xanthobilirubinic acid methyl ester

: 79719-28-1
3-{2-{3-(2-Carboxy-ethyl)-5-[3-ethyl-4-methyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-5-[3-ethyl-4-methyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 2,3,4,6-tetrachloro-1,4-benzoquinone (p-chloranil), HCOOH / CH₂Cl₂ / 42 h / Heating

2: 92 percent / NaBH₄ / tetrahydrofuran; methanol / 20 °C / ultrasound

3: 97 percent / 1 M aq. NaOH / tetrahydrofuran; methanol / 4 h / Heating

With sodium hydroxide; sodium tetrahydroborate; formic acid; chloranil; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1055/s-1992-26102