ethyl 2-(2,4,7-trimethyl-1H-indol-3-yl)acetate

Base Information

Chemical Name:ethyl 2-(2,4,7-trimethyl-1H-indol-3-yl)acetate
CAS No.:92652-15-8
Molecular Formula:C₁₅H₁₉NO₂
Molecular Weight:245.321
Hs Code.:
NSC Number:115150
DSSTox Substance ID:DTXSID60919028
Wikidata:Q82891417

Synonyms:ethyl 2-(2,4,7-trimethyl-1H-indol-3-yl)acetate;92652-15-8;NSC115150;SCHEMBL4561364;DTXSID60919028;NSC-115150;ethyl (2,4,7-trimethyl-1H-indol-3-yl)acetate

Suppliers and Price of ethyl 2-(2,4,7-trimethyl-1H-indol-3-yl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of ethyl 2-(2,4,7-trimethyl-1H-indol-3-yl)acetate

Chemical Property:

Vapor Pressure:3.98E-06mmHg at 25°C
Boiling Point:384.8°C at 760 mmHg
Flash Point:186.5°C
Density:1.115g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:245.141578849
Heavy Atom Count:18
Complexity:305

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CC1=C(NC2=C(C=CC(=C12)C)C)C

Technology Process of ethyl 2-(2,4,7-trimethyl-1H-indol-3-yl)acetate

There total 4 articles about ethyl 2-(2,4,7-trimethyl-1H-indol-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 539-88-8
4-oxopentanoic acid ethyl ester

: 613-85-4
(2,5-dimethylphenyl)hydrazine

: 92652-15-8
(2,4,7-trimethyl-indol-3-yl)-acetic acid ethyl ester

Guidance literature:: 4-oxopentanoic acid ethyl ester; (2,5-dimethylphenyl)hydrazine; With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; for 3h;

zinc(II) chloride; at 140 ℃;

Reference yield:

: 89-58-7
mononitro-p-xylene

: 92652-15-8
(2,4,7-trimethyl-indol-3-yl)-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate / Raney nickel / methanol; water / 2 h / 0 °C

2.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 5 °C

2.2: 0 - 20 °C

2.3: 0 °C

3.1: sodium hydrogencarbonate / dichloromethane; water / 3 h / 20 °C

3.2: 140 °C

With hydrogenchloride; sodium hydrogencarbonate; hydrazine hydrate; sodium nitrite; Raney nickel; In methanol; dichloromethane; water;

Reference yield:

: 95-78-3
2,5-Dimethylaniline

: 92652-15-8
(2,4,7-trimethyl-indol-3-yl)-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 5 °C

1.2: 0 - 20 °C

1.3: 0 °C

2.1: sodium hydrogencarbonate / dichloromethane; water / 3 h / 20 °C

2.2: 140 °C

With hydrogenchloride; sodium hydrogencarbonate; sodium nitrite; In dichloromethane; water;