propan-2-yl (Z)-2-methyl-3-phenylprop-2-enoate

Base Information

Chemical Name:propan-2-yl (Z)-2-methyl-3-phenylprop-2-enoate
CAS No.:7510-76-1
Molecular Formula:C13H16O2
Molecular Weight:204.2649
Hs Code.:
NSC Number:406215
DSSTox Substance ID:DTXSID30419702
Wikidata:Q82230862

Synonyms:NSC406215;7510-76-1;DTXSID30419702;NSC-406215

Suppliers and Price of propan-2-yl (Z)-2-methyl-3-phenylprop-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of propan-2-yl (Z)-2-methyl-3-phenylprop-2-enoate

Chemical Property:

Vapor Pressure:0.00202mmHg at 25°C
Boiling Point:290.8°C at 760 mmHg
Flash Point:150.8°C
Density:1.02g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:204.115029749
Heavy Atom Count:15
Complexity:235

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)OC(=O)C(=CC1=CC=CC=C1)C
Isomeric SMILES:CC(C)OC(=O)/C(=C\C1=CC=CC=C1)/C

Technology Process of propan-2-yl (Z)-2-methyl-3-phenylprop-2-enoate

There total 4 articles about propan-2-yl (Z)-2-methyl-3-phenylprop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1895-97-2
2-methyl-3-phenylacrylic acid

: 67-63-0,8013-70-5
isopropyl alcohol

: 7510-76-1
isopropyl α-methylcinnamate

Guidance literature:: With sulfuric acid; for 24h; Reflux; Inert atmosphere;
DOI:10.1002/chem.201200907

Reference yield: 81.0%

: 35086-87-4,38449-13-7
(E)-2-methyl-3-phenylacryloyl chloride

: 67-63-0,8013-70-5
isopropyl alcohol

: 7510-76-1
isopropyl α-methylcinnamate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/ejoc.201403220

Reference yield:

: 1895-97-2
2-methyl-3-phenylacrylic acid

: 7510-76-1
isopropyl α-methylcinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

2: dmap; triethylamine / dichloromethane / 0 - 20 °C

With dmap; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/ejoc.201403220