Technology Process of Benzenepropanoic acid, 2,4-bis(phenylmethoxy)-, phenylmethyl ester
There total 1 articles about Benzenepropanoic acid, 2,4-bis(phenylmethoxy)-, phenylmethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
Heating;
DOI:10.1021/jm020184n
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
DOI:10.1021/jm020184n
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 82 percent / LiAlH4 / tetrahydrofuran
2.1: 77 percent / pyridine / CH2Cl2 / 20 °C
3.1: 89 percent / LiBr / acetone / Heating
4.1: KOH / dimethylsulfoxide / 0.5 h
4.2: 58 percent / dimethylsulfoxide / 0.5 h / 50 °C
5.1: phosphorus oxychloride / acetonitrile / 1 h / 20 °C
5.2: acetonitrile / Heating
5.3: 61 percent / water / dioxane / 2 h / 50 °C
6.1: hydroxylamine hydrochloride; Et3N / acetonitrile / 45 °C
7.1: 15.64 g / phthalic anhydride / acetonitrile / Heating
8.1: 90 percent / H2 / 10percent Pd/C / ethyl acetate; ethanol / 5.5 h / 20 °C / 760.05 Torr
With
pyridine; potassium hydroxide; lithium aluminium tetrahydride; phthalic anhydride; hydroxylamine hydrochloride; hydrogen; triethylamine; lithium bromide; trichlorophosphate;
10percent Pd/C;
In
tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; acetone; acetonitrile;
5.2: Vilsmeier-Haack reaction;
DOI:10.1021/jm020184n
