1-methoxy-4-[3-(methylsulfinyl)-1,1-diphenylpropan-2-yl]benzene

Base Information

• Chemical Name: 1-methoxy-4-[3-(methylsulfinyl)-1,1-diphenylpropan-2-yl]benzene
• CAS No.: 13560-36-6
• Molecular Formula: C23H24 O2 S
• Molecular Weight: 364.5005
• Mol file: 13560-36-6.mol

Synonyms:Anisole,p-[1-[(methylsulfinyl)methyl]-2,2-diphenylethyl]- (7CI,8CI); NSC 80612

Chemical Property of 1-methoxy-4-[3-(methylsulfinyl)-1,1-diphenylpropan-2-yl]benzene

Chemical Property:

• Vapor Pressure: 6.52E-11mmHg at 25°C
• Boiling Point: 533.2°C at 760 mmHg
• Flash Point: 276.3°C
• Density: 1.16g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-methoxy-4-[3-(methylsulfinyl)-1,1-diphenylpropan-2-yl]benzene

There total 5 articles about 1-methoxy-4-[3-(methylsulfinyl)-1,1-diphenylpropan-2-yl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → 1-Methylsulfinyl-2-<4-methoxy-phenyl>-3,3-diphenyl-propan (13560-36-6)

Guidance literature:

Multi-step reaction with 2 steps

1: KOtBu / 1.5 h / 60 °C

2: KOtBu / dimethylsulfoxide

With potassium tert-butylate; In dimethyl sulfoxide;

DOI:10.1021/ja00872a044

Reference yield:

Diphenylmethane (101-81-5) + 1-(2-methanesulfinylvinyl)-4-methoxybenzene (13350-30-6) → 1-Methylsulfinyl-2-<4-methoxy-phenyl>-3,3-diphenyl-propan (13560-36-6)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide;

DOI:10.1021/ja00872a044

Reference yield:

Diphenylmethane (101-81-5) + 4-methoxy-benzaldehyde (123-11-5) + dimethyl sulfoxide (67-68-5,8070-53-9) → 1,1-diphenyl-2-(p-methoxyphenyl)propene (13560-37-7) + 1-Methylsulfinyl-2-<4-methoxy-phenyl>-3,3-diphenyl-propan (13560-36-6)

Guidance literature:

With potassium tert-butylate; at 60 ℃;

DOI:10.1021/ja00872a044

upstream raw materials:

Diphenylmethane

1-(2-methanesulfinylvinyl)-4-methoxybenzene

4-methoxy-benzaldehyde

dimethyl sulfoxide

Downstream raw materials:

3.3-Diphenyl-2-<4-methoxy-phenyl>-propen-(1)

1-Methylsulfonyl-2-<4-methoxy-phenyl>-3,3-diphenyl-propan

1,1-diphenyl-2-(p-methoxyphenyl)propene