1-Phenylnaphthalen-2-ol

Base Information

• Chemical Name: 1-Phenylnaphthalen-2-ol
• CAS No.: 4919-96-4
• Molecular Formula: C16H12O
• Molecular Weight: 220.271
• DSSTox Substance ID: DTXSID50459089
• Nikkaji Number: J951.315I
• Wikidata: Q82282701
• Mol file: 4919-96-4.mol

Synonyms:1-phenylnaphthalen-2-ol;4919-96-4;1-phenyl-2-naphthol;2-Naphthalenol, 1-phenyl-;1-phenyl-naphthalen-2-ol;SCHEMBL619730;DTXSID50459089;MFCD32667031;E87051

Chemical Property of 1-Phenylnaphthalen-2-ol

Chemical Property:

• XLogP3: 4.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 220.088815002
• Heavy Atom Count: 17
• Complexity: 244

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=C(C=CC3=CC=CC=C32)O

Technology Process of 1-Phenylnaphthalen-2-ol

There total 54 articles about 1-Phenylnaphthalen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-bromo-2-naphthol (573-97-7) + phenylboronic acid (98-80-6) → 1-phenylnaphthalen-2-ol (4919-96-4)

Guidance literature:

With 2′-(di-o-anisylphosphanyl)biphenyl-2-yl camphanate; palladium diacetate; potassium carbonate; In water; toluene; at 105 - 110 ℃; for 0.333333h; Reagent/catalyst; Inert atmosphere; Microwave irradiation;

DOI:10.1002/ejic.201700282

Reference yield: 94.0%

tetraphenyl-bismuth trifluoroacetate (83566-43-2) + β-naphthol (135-19-3) → 1-phenylnaphthalen-2-ol (4919-96-4)

Guidance literature:

With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; In benzene; Ambient temperature;

Reference yield: 91.0%

5-tert-butyl-5-phenyl-5H-benzo[c]naphtho[1,2-e][1,2]oxasiline (1178513-94-4) → 1-phenylnaphthalen-2-ol (4919-96-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 70 ℃;

DOI:10.1021/ja904791y

upstream raw materials:

3-Butyloxy-2,2-diphenyl-cyclobutanon-⁽¹⁾

ethyl-(1-phenyl-[2]naphthyl)-ether

4-chloro-1-phenyl-2-naphthol

pentaphenylbismuth

Downstream raw materials:

2-methoxy-1-phenylnaphthalene

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