Benzoic acid, 3-[3-[bis(phenylmethoxy)methyl]-6-chloro-1,5,8-trimethoxy-2-naphthalen yl]-4-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-6-methyl-, methyl ester

Base Information

Chemical Name:Benzoic acid, 3-[3-[bis(phenylmethoxy)methyl]-6-chloro-1,5,8-trimethoxy-2-naphthalen yl]-4-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-6-methyl-, methyl ester
CAS No.:492453-49-3
Molecular Formula:C55H57ClO9Si
Molecular Weight:925.591
Hs Code.:

Benzoic acid,
3-[3-[bis(phenylmethoxy)methyl]-6-chloro-1,5,8-trimethoxy-2-naphthalen
yl]-4-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-6-methyl-,
methyl ester

Synonyms:

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Chemical Property of Benzoic acid, 3-[3-[bis(phenylmethoxy)methyl]-6-chloro-1,5,8-trimethoxy-2-naphthalen yl]-4-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-6-methyl-, methyl ester

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Technology Process of Benzoic acid, 3-[3-[bis(phenylmethoxy)methyl]-6-chloro-1,5,8-trimethoxy-2-naphthalen yl]-4-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-6-methyl-, methyl ester

There total 4 articles about Benzoic acid, 3-[3-[bis(phenylmethoxy)methyl]-6-chloro-1,5,8-trimethoxy-2-naphthalen yl]-4-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-6-methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 14642-79-6
benzyloxy-trimethylsilane

: 492453-48-2
4-(tert-butyl-diphenyl-silanyloxymethyl)-3-(6-chloro-3-formyl-1,5,8-trimethoxy-naphthalen-2-yl)-2-methoxy-6-methyl-benzoic acid methyl ester

: 492453-49-3
3-[3-(bis-benzyloxy-methyl)-6-chloro-1,5,8-trimethoxy-naphthalen-2-yl]-4-(tert-butyl-diphenyl-silanyloxymethyl)-2-methoxy-6-methyl-benzoic acid methyl ester

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate;
DOI:10.1016/S0040-4039(02)01608-8

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 492453-49-3
3-[3-(bis-benzyloxy-methyl)-6-chloro-1,5,8-trimethoxy-naphthalen-2-yl]-4-(tert-butyl-diphenyl-silanyloxymethyl)-2-methoxy-6-methyl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / imidazole / dimethylformamide

2: 96 percent / TMSOTf

With 1H-imidazole; trimethylsilyl trifluoromethanesulfonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)01608-8

Reference yield:

: 492453-59-5
3-(6-chloro-3-formyl-1,5,8-trimethoxy-naphthalen-2-yl)-2-methoxy-4-methoxymethoxymethyl-6-methyl-benzoic acid methyl ester

: 492453-49-3
3-[3-(bis-benzyloxy-methyl)-6-chloro-1,5,8-trimethoxy-naphthalen-2-yl]-4-(tert-butyl-diphenyl-silanyloxymethyl)-2-methoxy-6-methyl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / aq. HCl / 1,2-dimethoxy-ethane / 40 °C

2: 100 percent / imidazole / dimethylformamide

3: 96 percent / TMSOTf

With 1H-imidazole; hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)01608-8