3-acetyl-1-[2-(1H-indol-3-yl)ethyl]pyridinium

Base Information

Chemical Name:3-acetyl-1-[2-(1H-indol-3-yl)ethyl]pyridinium
CAS No.:2883-99-0
Molecular Formula:Br*C₁₇H₁₇N₂O
Molecular Weight:345.239
Hs Code.:
Mol file:2883-99-0.mol

Synonyms:3-Acetyl-1-(2-indol-3-ylethyl)pyridiniumbromide (7CI); Pyridinium, 3-acetyl-1-(2-indol-3-ylethyl)-, bromide (8CI);Pyridinium, 3-acetyl-1-[2-(1H-indol-3-yl)ethyl]-, bromide (9CI)

Suppliers and Price of 3-acetyl-1-[2-(1H-indol-3-yl)ethyl]pyridinium

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 6 raw suppliers

Chemical Property of 3-acetyl-1-[2-(1H-indol-3-yl)ethyl]pyridinium

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-acetyl-1-[2-(1H-indol-3-yl)ethyl]pyridinium

There total 2 articles about 3-acetyl-1-[2-(1H-indol-3-yl)ethyl]pyridinium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 350-03-8
methyl-3-pyridylketone

: 3389-21-7
3-(2-bromoethyl)-1H-indole

: 2883-99-0
3-Acetyl-1-[2-(1H-indol-3-yl)-ethyl]-pyridinium; bromide

Guidance literature:: In diethyl ether; at 100 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201703178

Reference yield:

: 2883-99-0
3-Acetyl-1-[2-(1H-indol-3-yl)-ethyl]-pyridinium; bromide

Guidance literature:: Tryptophylbromid, Nicotinmethylketon;
DOI:10.1021/ja00428a044

Reference yield:

: 2883-99-0
3-Acetyl-1-[2-(1H-indol-3-yl)-ethyl]-pyridinium; bromide

: 20361-93-7,21067-29-8,24196-07-4,55529-55-0,60383-90-6,62058-41-7,63569-17-5,63597-39-7,69349-84-4,81737-76-0,107741-10-6,107741-11-7
(7aS,8S,11S,11aR,12aS)-10-Hydroxy-8-methyl-5,6,7a,8,10,11,11a,12,12a,13-decahydro-7H-9-oxa-6a,13-diaza-indeno[2,1-a]anthracene-11-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 1.) from -15 deg C to RT 3-5 h, 2.) RT, 20 h

2: 48 percent / NaBH₄ / acetic acid; methanol / 23 h

With sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; acetic acid;