Technology Process of Benzoic acid,
4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-2-methyl-
, methyl ester
There total 3 articles about Benzoic acid,
4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-2-methyl-
, methyl ester which
guide to synthetic route it.
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synthetic route:
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-
495388-46-0
4-((E)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluoro-dec-1-enyl)-2-methyl-benzoic acid methyl ester
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-
495388-47-1
4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-2-methyl-benzoic acid methyl ester
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
for 3h;
under 2250.18 Torr;
DOI:10.1016/S0040-4039(02)01723-9
-
-
495388-47-1
4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-2-methyl-benzoic acid methyl ester
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 72 percent / NaOAc / Herrmann-Beller catalyst / dimethylformamide / 14 h / 125 °C
2: 88 percent / H2 / Pd/C / 3 h / 2250.18 Torr
With
hydrogen; sodium acetate;
palladium on activated charcoal; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II);
In
N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)01723-9
-
-
495388-47-1
4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-2-methyl-benzoic acid methyl ester
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 72 percent / NaOAc / Herrmann-Beller catalyst / dimethylformamide / 14 h / 125 °C
2: 88 percent / H2 / Pd/C / 3 h / 2250.18 Torr
With
hydrogen; sodium acetate;
palladium on activated charcoal; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II);
In
N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)01723-9