3-Butenenitrile, 2-(acetyloxy)-3-methyl-4-(3-phenoxyphenyl)-, (R-(E))-

Base Information

Chemical Name:3-Butenenitrile, 2-(acetyloxy)-3-methyl-4-(3-phenoxyphenyl)-, (R-(E))-
CAS No.:99603-88-0
Molecular Formula:C₁₉H₁₇NO₃
Molecular Weight:307.349
Hs Code.:

Synonyms:3-Butenenitrile, 2-(acetyloxy)-3-methyl-4-(3-phenoxyphenyl)-, (R-(E))-;99603-88-0

Suppliers and Price of 3-Butenenitrile, 2-(acetyloxy)-3-methyl-4-(3-phenoxyphenyl)-, (R-(E))-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Butenenitrile, 2-(acetyloxy)-3-methyl-4-(3-phenoxyphenyl)-, (R-(E))-

Chemical Property:

Vapor Pressure:1.13E-09mmHg at 25°C
Boiling Point:488°C at 760 mmHg
Flash Point:212°C
Density:1.163g/cm³
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:307.12084340
Heavy Atom Count:23
Complexity:470

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CC1=CC(=CC=C1)OC2=CC=CC=C2)C(C#N)OC(=O)C
Isomeric SMILES:C/C(=C\C1=CC(=CC=C1)OC2=CC=CC=C2)/[C@H](C#N)OC(=O)C

Technology Process of 3-Butenenitrile, 2-(acetyloxy)-3-methyl-4-(3-phenoxyphenyl)-, (R-(E))-

There total 1 articles about 3-Butenenitrile, 2-(acetyloxy)-3-methyl-4-(3-phenoxyphenyl)-, (R-(E))- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.5%

: 99566-47-9,99603-89-1
(E)-(+/-)-1-cyano-2-methyl-3-(3-phenoxyphenyl)-2-propenyl acetate

: 99566-48-0
(E)-(S)-2-Hydroxy-3-methyl-4-(3-phenoxy-phenyl)-but-3-enenitrile

: 99603-88-0,99566-47-9,99603-89-1
(E)-(R)-1-cyano-2-methyl-3-(3-phenoxyphenyl)-2-propenyl acetate

Guidance literature:: With lipase Amano P; at 28 ℃; for 16h;

Reference yield: 79.2%

: 67-56-1
methanol

: 99603-88-0,99566-47-9,99603-89-1
(E)-(R)-1-cyano-2-methyl-3-(3-phenoxyphenyl)-2-propenyl acetate

: 99566-49-1
(E)-(R)-methyl 2-hydroxy-3-methyl-4-(3-phenoxyphenyl)-3-butenoate

Guidance literature:: In hydrogenchloride; methanol; for 72h; Ambient temperature;

Reference yield:

: 99603-88-0,99566-47-9,99603-89-1
(E)-(R)-1-cyano-2-methyl-3-(3-phenoxyphenyl)-2-propenyl acetate

: 99566-51-5
(E)-(R)-3-methyl-4-(3-phenoxyphenyl)-3-buten-1,2-diol acetonide

Guidance literature:: Multi-step reaction with 3 steps

1: 79.2 percent / HCl; methanol / 72 h / Ambient temperature

2: 1.18 g / lithium aluminum hydride / diethyl ether / 1 h / 20 °C

3: 1.3 g / p-toluenesulfonic acid

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In hydrogenchloride; methanol; diethyl ether;