t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

Base Information

Chemical Name:t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate
CAS No.:1253511-94-2
Molecular Formula:C₂₀H₂₃N₇O₃
Molecular Weight:409.448
Hs Code.:

Synonyms:t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

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Chemical Property of t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

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Technology Process of t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

There total 3 articles about t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 888322-11-0
2-[bis(tert-butoxycarbonyl)amino]-6-(bromomethyl)pyridine

: N-hydroxy-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

: 500207-04-5
tert-butyl N-[6-({[(Z)-[(1-methyl-1H-1,2,3,4-tetrazol-5-yl)(phenyl)methylidene]amino]oxy}methyl)pyridin-2-yl]carbamate

: 1253511-94-2
t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In water; at 20 ℃; for 2h; Overall yield = 77.1 %; Overall yield = 6.1 g;

Reference yield:

: 1824-81-3
2-Amino-6-methylpyridine

: 500207-04-5
tert-butyl N-[6-({[(Z)-[(1-methyl-1H-1,2,3,4-tetrazol-5-yl)(phenyl)methylidene]amino]oxy}methyl)pyridin-2-yl]carbamate

: 1253511-94-2
t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; pyridine / N,N-dimethyl-formamide / 5 h / 90 °C

2.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile) / chlorobenzene / 1 h / 20 - 90 °C

2.2: 16.5 h / 10 - 20 °C

3.1: tetrabutylammomium bromide; sodium hydroxide / water / 2 h / 20 °C

With pyridine; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; triethylamine; sodium hydroxide; In water; N,N-dimethyl-formamide; chlorobenzene;

Reference yield:

: 888322-04-1
t-butyl t-butoxycarbonyl-(6-methyl-pyridin-2-yl)-carbamate

: 500207-04-5
tert-butyl N-[6-({[(Z)-[(1-methyl-1H-1,2,3,4-tetrazol-5-yl)(phenyl)methylidene]amino]oxy}methyl)pyridin-2-yl]carbamate

: 1253511-94-2
t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile) / chlorobenzene / 1 h / 20 - 90 °C

1.2: 16.5 h / 10 - 20 °C

2.1: tetrabutylammomium bromide; sodium hydroxide / water / 2 h / 20 °C

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; sodium hydroxide; In water; chlorobenzene;