{5-[(Benzyloxy)methyl]-2,2-dimethyl-1,3-dioxan-5-yl}methanol

Base Information

Chemical Name:{5-[(Benzyloxy)methyl]-2,2-dimethyl-1,3-dioxan-5-yl}methanol
CAS No.:500358-89-4
Molecular Formula:C15H22O4
Molecular Weight:266.337
Hs Code.:
DSSTox Substance ID:DTXSID00514536
Wikidata:Q82374920

Synonyms:500358-89-4;DTXSID00514536;{5-[(Benzyloxy)methyl]-2,2-dimethyl-1,3-dioxan-5-yl}methanol

Suppliers and Price of {5-[(Benzyloxy)methyl]-2,2-dimethyl-1,3-dioxan-5-yl}methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of {5-[(Benzyloxy)methyl]-2,2-dimethyl-1,3-dioxan-5-yl}methanol

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:266.15180918
Heavy Atom Count:19
Complexity:261

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(OCC(CO1)(CO)COCC2=CC=CC=C2)C

Technology Process of {5-[(Benzyloxy)methyl]-2,2-dimethyl-1,3-dioxan-5-yl}methanol

There total 2 articles about {5-[(Benzyloxy)methyl]-2,2-dimethyl-1,3-dioxan-5-yl}methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 130147-42-1
2-<(benzyloxy)methyl>-2-(hydroxymethyl)-1,3-propanediol

: 77-76-9
2,2-dimethoxy-propane

: 500358-89-4
5-(benzyloxymethyl)-5-(hydroxymethyl)-2,2-dimethyl-1,3-dioxane

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1016/S0040-4020(02)01067-0

Reference yield:

: 500358-88-3
2-(benzyloxymethyl)-2-(toluene-4-sulfonyloxymethyl)-1,3-propanediol

: 500358-89-4
5-(benzyloxymethyl)-5-(hydroxymethyl)-2,2-dimethyl-1,3-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / NaHCO₃; NaN₃; aliquat / toluene; H₂O / 16 h / Heating

2: 82 percent / p-toluenesulfonic acid / acetonitrile / 1 h / 20 °C

With sodium azide; Aliquat; sodium hydrogencarbonate; toluene-4-sulfonic acid; In water; toluene; acetonitrile;
DOI:10.1016/S0040-4020(02)01067-0