Phosphonium, (2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)diphenyl(phenylmethyl)-, bromide

Base Information

Chemical Name:Phosphonium, (2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)diphenyl(phenylmethyl)-, bromide
CAS No.:134403-72-8
Molecular Formula:Br*C₃₃H₃₆O₅P
Molecular Weight:623.524
Hs Code.:
DSSTox Substance ID:DTXSID10928605
Mol file:134403-72-8.mol

Synonyms:134403-72-8;Phosphonium, (2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)diphenyl(phenylmethyl)-, bromide;C33H36O5P.Br;C33-H36-O5-P.Br;DTXSID10928605;LS-106928;Benzyl(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)diphenylphosphanium bromide;Benzyl(2,3,5,6,8,9,11,12-octahydrobenzo[b][1,4,7,10,13]pentaoxacyclopentadecin-15-yl)diphenylphosphonium bromide;Benzyl(2,3,5,6,8,9,11,12-octahydrobenzo[b][1,4,7,10,13]pentaoxacyclopentadecin-15-yl)diphenylphosphoniumbromide

Suppliers and Price of Phosphonium, (2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)diphenyl(phenylmethyl)-, bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Phosphonium, (2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)diphenyl(phenylmethyl)-, bromide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:622.14837
Heavy Atom Count:40
Complexity:641

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCOC2=C(C=C(C=C2)[P+](CC3=CC=CC=C3)(C4=CC=CC=C4)C5=CC=CC=C5)OCCOCCO1.[Br-]

Technology Process of Phosphonium, (2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)diphenyl(phenylmethyl)-, bromide

There total 1 articles about Phosphonium, (2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)diphenyl(phenylmethyl)-, bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 60835-72-5
4'-bromobenzo-15-crown-5-ether

: 7650-91-1
benzyldiphenylphosphane

: 134403-72-8
4-(Benzyldiphenylphosphonio)benzo-15-crown-5 bromide

Guidance literature:: With nickel dibromide; In benzonitrile;

Reference yield:

: 134403-72-8
4-(Benzyldiphenylphosphonio)benzo-15-crown-5 bromide

: 134988-67-3
4-(diphenylphosphinothioyl)benzo-15-crown-5

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / LiAlH₄ / tetrahydrofuran / 15 h / Heating

2: 90 percent / sulfur / benzene / 6 h

With lithium aluminium tetrahydride; sulfur; In tetrahydrofuran; benzene;