phosphorous dibromide fluoride

Base Information

• Chemical Name: phosphorous dibromide fluoride
• CAS No.: 15597-39-4
• Molecular Formula: Br2FP
• Molecular Weight: 209.78
• Mol file: 15597-39-4.mol

Synonyms:

Chemical Property of phosphorous dibromide fluoride

Chemical Property:

• Boiling Point: 78.31°C (estimate)
• PSA: 13.59000
• LogP: 2.97260

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of phosphorous dibromide fluoride

There total 2 articles about phosphorous dibromide fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

antimony(III) fluoride (7783-56-4) + phosphorus tribromide (7789-60-8) → PBr2F (15597-39-4) + bromodifluorophosphine (15597-40-7) + trifluorophosphane (7783-55-3)

Guidance literature:

bromine; In neat (no solvent); fluorination of PBr3 with SbF3 using Br2 as catalyst;;

DOI:10.1021/ja01265a102

Reference yield:

calcium fluoride + phosphorus tribromide (7789-60-8) → PBr2F (15597-39-4) + bromodifluorophosphine (15597-40-7) + trifluorophosphane (7783-55-3)

Guidance literature:

In neat (no solvent); fluorination with CaF2 at 200°C;;

DOI:10.1021/ja01265a102

Reference yield:

PBr2F (15597-39-4) → phosphorus + hydrogen fluoride (7664-39-3,12381-92-9,32057-09-3,74835-82-8) + hydrogen bromide (10035-10-6,12258-64-9)

Guidance literature:

With H₂O; In water; easily hydrolyzed;;

DOI:10.1021/ja01265a102

upstream raw materials:

antimony(III) fluoride

phosphorus tribromide

Downstream raw materials:

hydrogen fluoride

hydrogen bromide

trifluorophosphane

phosphorus fluoride dichloride

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